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GCMS analysis results for sample AE09578, May 2002

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Laboratory report showing GC/MS analysis results for sample AE09578 including surrogate recovery data on May 16, 2002.

NYC-WTC_000023316–000023326

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000023325
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY0 902\9578.D Vial: 6 Acq On 9 May 2002 7:14 pm Operator: Sample GC/MS SCAN 5/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Anthracene-dlO- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 25.72 0.47 ug/1 41378 Phenanthrene-dl0 25.58 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene/dlO- 7 001719-06-8 70 188 C14D10 2 Phenanthrene-diO / 001517-22-2 59 188 C14D10 3 4H-Pyrido [1,2-a]pyrimidin-4-one, 3- 188 C11H12N2O 057773-19-0 23 4 1,4-Naphthalenedione, 2-hydroxy-3-m 188 C11H803 000483-55-6 9 Abundance Scan 2256 (25.717 min): 9578.D (-) m/z 188.15 100.00%| 188

5000 44 80 94 .......... ...........................

m/z-> 30 —3++ TT+T-HH 40 52 50 60 66 70 80 ।" " i TH I ' 1 ’ 1 I 160 TPTP TIT 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 m/z 44.05 32.25% Abundance #19957: Anthracene-d10- 1118

5000 25.40 25.60 25.80 26.00 m/ Z 40.05 29.25% 160 m/z-> 30 466, 1 q 40 r 50 60 70 80 T’T 90 100 110 120 130 140 150 160 170 180 190

— —e Abundance #19958: Phenanthrene-d10 188 AMAMCP 25.40 25.60 25.80 26.00 5000 m/ z 94.10 20.71

94 80 160 66 | 1mTT 111■■।■i■••-1. ■ । ।>111111 > > ...... I*... rn/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19873:4H-Pyrido[1,2-a]pyrimidin-4-one, 3-ethyl-6-methyl- - 145 188 25,40 25.60 25.80 26.00 173 m/z 189.15 19.98%| 5000 92

65 159

m/z—> I 119 132 TICTTITTTTTIPWTTTTTTTTT ■ " i' " ' r " 11' ■ " i " " i" 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 | +.. Hm H TT‘ ....................................... 25.40 25.60 25.80 26,00

9578.D GCMS0510.M Fri May 10 13:59:18 2002 Page 3

NYC-WTC_000023325

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NYC-WTC_000023325Source: NYC Law Department, mirrored locally

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