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GCMS analysis results for sample AE09578, May 2002

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Laboratory report showing GC/MS analysis results for sample AE09578 including surrogate recovery data on May 16, 2002.

NYC-WTC_000023316–000023326

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000023324
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY0 902\9578.D Vial: 6 Acq On 9 May 2002 7:14 pm Operator: Sample GC/MS SCAN 5/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.79 2.08 ug/1 177488 Naphthalene-d8 15.83 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclope: asiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Pheneth lamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 40 3 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 4 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 38 Abundance Scan 1064 (14.794 min): 9578. D (-) m/ z 73.10 100.00%| 73

5000 267 355 .. ................... . 45 14,40 14.60 14.80 15.00 15.20 — 108 154 193 223 323 THtm—fr rr-r m/z 267.05 32.17% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 1 i ■ ■ 1 ' i 14.40 14.60 14.80 15.00 15.20 m/z 355.10 28.76%! — 323, TTT ............................ 207 17.l miz—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 10 — 14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.10 10.19%|

m/z-> Abundance Lu 50 , 147 193 267294 1 1 । 1 1 1 1 i 1 1 1 1 i ■ 1 1 1 i 1 1 1 ''i 1 1 1 ■ i ' 1 1 1 i 1 1 1 1 i 1 1 1 '[ 1 1 1 1 I 1 1 100 150 200 250 300 350 400 #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 450 500 550 73 14.40 14,60 14,80 15.00 15.20 355 m/z 267.95 8.69%

5000

45 | ..... 208 251 281 .. 386... 458 548 ‘ I ' 11 ' ' i ■ ■ ■ ■ i ■ ■ m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

9578.D GCMS0510.M Fri May 10 13:59:17 2002 Page 2

NYC-WTC_000023324

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NYC-WTC_000023324Source: NYC Law Department, mirrored locally

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