GCMS analysis results for sample AE10773, May 2002

Machine-extracted title · confidence 50%

Gas chromatography-mass spectrometry report for sample AE10773 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000045859–000045868

Folder label: “GCMS X 5/6/02 A 5/11/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAY1002\10773.D Vial: 17 Acq On : 11 May 2002 4:40 am Operator: Sample : GC/MS SCAN 5/6 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.77 0.46 ug/1 43255 Naphthalene-d8 15.80

Hit# Of/ 5 Tentative ID MW MolForm CAS# Qual

1 opentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 80 2 enethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 3/N-(Trifluoroacetyl)-N,0,0',O' '-tetr 553 C22H42F3NO4Si4 000000-00-0 38 4 Benzeneethanamine, N- [(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 1062 (14.770 min): 10773.D (-) m/z 73.10 100.00% 73

5000 267 355 V T ■ ■ i ■

14.40 14.60 14.80 15.00 15.20 45 154 193 323 ' '11 ' ‘ TImomer । ■ । T ‘1 r r*r t T i" 1“r I r । ■ 1 ■ i m/z 267.05 37.56% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 111 1 i 11 r'I 1 14.40 14.60 14.80 15.00 15.20 m/z 355.10 34.29% 207 • 7 ■ * ■ ■ 323 । • ■■ ■ । ■ ■ ■ ■ । • ■ ■ ■ । ■ ■ ■ ■ । ■ ' ■ ■ । ■ —t m/z->______ 50 100 150200 250 300 350 400 450 500 550 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 TI II 14.40 14.60 14.80 15.00 15.20 5000 355 m/ Z 356.10 12.60% 44 1 147 193 267 294 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi II I ' ' ' ■ i 1 1 r ' i ' 73 14.40 14.60 14.80 15.00 15.20 m/z 267.95 9.65% 355 5000

45 1 ii 1 1 i 1 ■ ■ ‘I‘ 147 193 267 538 1 । 1 ' 1 1 । 1 1 ■ 1 । 1 ■ ■ ' । 1 1 1 i ' ■ ■ 1 i ' ' ■ 1 ' i ■ ’ ’ ' i ' m/z— > 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

10773.D GCMS0510.M Mon May 13 14:27:21 2002 Page 2

NYC-WTC_000045867

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000045867Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS reference results for sample AE10772, May 2002 · Box DEP Box 25

NYC-WTC_000045849

Gas chromatography-mass spectrometry reference report for sample AE10772 listing measured values and detection limits.

1 shared topics · Same agency, volume and box · similarity 0.999