GCMS analysis results for sample AE08682, April 23, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1202\8682.D Vial: 14 Acq On : 15 Apr 2002 8:49 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.83 0.42 ug/1 69505 Naphthalene-d8 15.86 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 000541-02-6 50 370 C10H3005Si5 2 Phenethylamine, N-methyl-.beta. ,3,4 399 C18H37NO3Si3 010538-85-9 47 3 Silane, [ [4-[1, 2-bis [ (trimethylsily 458 C20H42O4Si4 056114-62-6 47 4 Benzeneethamamine, N~ [ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 Abundance Scan 1066 (14.833 min): 8682.D (-) m/z 73.00 100.00% 73

267 355 5000

45 125 154 193 237 14.60 14.80 15.00 15.20 - ■ i ' ■ ■ ■ i • ■ ■ • i • 1 ■ ■ i ■ ,32.1 m/z 355.05 57.34% miz-> 50 100 150 200 250 300 350 400 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 .................... 5000 ' • I 1 ■ ' ‘ ‘ I ‘ ' I • ‘ 14.60 14.80 15.00 15.20 m/z 267.00 51.87% 323 J ' ■ i mz-> 50 100 150 200 250 300 350 400 Abundance #74238: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 355 73 14.60 14.80 15.00 15.20 5000 m/z 356.05 19.85%

44 .147 179 265 294 I 384 miz-> -4 50 100 ‘ ' 150 200 250 '360' 350 '460' Abundance #74513: Silane, [4-[1,2-bis[(trimethylsilyl)oxy]ethyl]-1,2 355 ■ ■ i ■ ‘ ■ ■ i ■ ■ ■ • i ■ ■ 14.60 14.80 15.00 15.20 m/z 267.90 14.28% 5000 73

45 147 179 207 251 281 443 __________ TI- Bn ■ ■ i ■ ■ ’**1*’IS mfz-> 50 100 150 200 250 300 350 400 14,60 14.80 15.00 15.20

8682.D GCMS0412.M Tue Apr 16 15:42:32 2002 Page 2

NYC-WTC_000048865