NYC-WTC_000011942
Technical record of GCMS calibration data for TCLP analysis using sample vial 13 from March 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
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GCMS calibration table for TCLP analysis, March 2002
Machine-extracted title · confidence 100%Technical record of GCMS calibration data for TCLP analysis using sample vial 14 from March 28, 2002.
NYC-WTC_000011949–000011955Folder label: “GCMS X 2/28/02 A 3/26/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\MAR2502\4387.D Vial: 14 Acq On : 25 Mar 2002 11:01 pm Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
14.85 2.59 ug/1 428523 Naphthalene-d8 15.88
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 cyclopentiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 87 2 Phenethylamine, N-methyl-.beta. , 3,4 399 C18H37NO3Si3 010538-85-9 38 3 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38 4 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 Abundance Scan 1068 (14.846 min) 4387.D (-) m/z 73.00 100.00% 73
5000 267 355 T-r-p-r ‘*I***I* ■ 45 1...... 108 133 154 177 193208223 251 14.60 14.80 15,00 15.20 293 323339 L ■' i “ 'T"^ I n " ITtpnpupmg- 1’1523111m1umutntI m/z 267.00 42.91% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 _ .......... 5000 14.60 14.80 15.00 15.20 m/z 355.05 41.26% 191207 251 , 323339 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance 478239 Plon ' ti site ■ 73 - 14.60 14.80 15.00 15.20 5000 355 m/z 356.0 14.79% 44 88 130147 193 267 294 f m/z-> 40 60 80 100 120 140 160 180 260' '226' '240 260 280 '366' '320 '340 360 ''' Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsiiyl)oxy]-, trimet 73 14.60 14.80 15.00 15.20 m/z 268.00 11.78% 5000 355 45 133149 193 , 223 281 340 370 i ‘ ■ i ■ ‘ ' i ■ “ ■ i TTp, 111 i* l AaT—osri .... I i " " i ■1 ■ • i “ “ i' "11" “ i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20
4387.D GCMS0308.M Thu Mar 28 12:30:13 2002 Page 1
NYC-WTC_000011954
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