GCMS results for sample AE04413, April 2002

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Laboratory report documenting GCMS analysis of environmental sample AE04413 conducted on April 3, 2002.

NYC-WTC_000011905–000011915

Folder label: “GCMS X 2/28/02 A 3/26/02”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\MAR2502\4413.D Vial: 19 Acq On : 26 Mar 2002 3:57 am Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.84 2.64 ug/1 476281 Naphthalene-d8 15.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 000541-02-6 64 370 C10H3005Si5 2 Phenethylamine, N-methyl-. beta. ,3,4 399 C18H37NO3Si3 010538-85-9 38 3 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 38 4 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 Abundance Scan 1067 (14.844 min): 4413.D (-) m/z 73.00 100.00% 73

5000 267 355 ■ ‘ i ■ ■ ................ ‘ 1 * I ‘ ‘ * I 1 ' 45 177 193208223 251 14.60 14.80 15.00 15.20 ’ I’ —89. 1981‘ l133‘ I ‘ 154 ‘ 293 ‘ ‘323339 1 ■ ■ j ■ > • ' l1 ‘ ■ 'l “ ‘" I “ “ I fl ‘ ‘ ‘ । <4.11 ‘i 11 i ।. T . । i m/z 267.00 44.01 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.60 14.80 15.00 15.20 m/z 355.05 39.75 , | ........ 191 207.. 251... 323339 .1.. m/z-> 40 60. 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ' Abundancei 2ra27t to ntne - a jhobew,3d-trsanomatms,t 73 ....... /...... ..

14.60 14.80 15.00 15.20 5000 355 14.13% 44 ... ’ 88 193 130147 267 294 ‘ ""Ut TT—0101m0mm—umpanmar TWI171—mmPunpmBgont m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet 73 355 14.60 14.80 15.00 15.20 m/z 268.00 11.44% 5000

147 267 47 208! 249 370 ‘' I' ‘1 ‘ i “ “ i “ " i “ ' • l “ “ I •' “ i' ‘ “ I ‘ i|i ‘ "I‘“i ‘ rrtn l ii 283 Al 1′1′4 [ l i T| ■>i ■ 111 > <।> I I TT miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 . 14.60 14.80 15.0 15.20

4413.D GCMS0308.M Thu Mar 28 12:36:44 2002 Page 3

NYC-WTC_000011914

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NYC-WTC_000011914Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE04128, April 2002 · Box DEP Box 14

NYC-WTC_000011767

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