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GCMS analysis results for sample AE04388, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AE04388 conducted on April 3, 2002.

NYC-WTC_000011857–000011867

Folder label: “GCMS X 2/28/02 A 3/26/02

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Scanned page image, NYC-WTC_000011864
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2502\4388.D Vial: 15 Acq On : 26 Mar 2002 12:01 am Operator: Sample : gc/ms scan 2/28 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.85 1.83 ug/1 318239 Naphthalene-d8 15.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 3 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4 Benzoic acid. 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 32 Abundance Scan 1068 (14.847 min): 4388.D (-) m/z 73.00 100.00% 73

5000 267 355 -r-r-j-r-T .... 45 133 154 , 193 223 249 323 I 14.60 14.80 15.00 15.20 np 1, —n,—B—108 —8E*HmgTTmT "i“ 17 .293., mmmmmmppp m/z 267.00 46.26% miz-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 , ................................... 5000 14.60 14.80 15.00 15.20 m/z 355.05 45.07% 207 249 [ 323 TCTagamompapar m/z~> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance iwr. 0 3. -riftarethy! 73 ■ 11 1 । • ■ ■ ■ । ■ i • ■ 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 16.08% 44 147 193 267 294 TOpnpap miz-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #57357: Noradrenaline, tetra-TMS 73 14.60 14.80 15.00 15.20 m/z 268.00 12.12% 5000 102 355

45 147 । .... j.,,, ।,... ।,.,,442 TTmgg—gM—mpaug .!., 111 >... ।.... ।.... ।.... ।< lT| ।. "i1" m/z->40 60 80 100120140160180200220240260280300320340360380400420440 14.60 14.80 15.00 15.20

4388.D GCMS0308.M Thu Mar 28 12:31:05 2002 Page 1

NYC-WTC_000011864

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NYC-WTC_000011864Source: NYC Law Department, mirrored locally

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