GCMS sample analysis report AE08435, Apr 18 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR12 02\84 3 5.D Vial: 24 Acq On : 16 Apr 2002 6:37 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************************* * * Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.83 3.57 ug/1 638342 Naphthalene-d8 15.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Phenethylamine, N-methyl - . beta . , 3,4 399 C18H37NO3Si3 010538-85-9 38 3 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38 4 Noradrenaline, tetra-TMS____________ 457 C20H43NO3Si4 000000-00-0 37 Abundance Scan 1066 (14.829 min): 8435.D (-) m/z 73.00 100.00% 73

5000- 267 355

—। ........ r i / ! ! i t i < > | i i i ......... । > ■ i<i i | |

m/z-> 45 — i unu f 89 108 133 154 177193 223 251 | —mmnmmOTenummam i "293 111 323339 TTTT 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 4 m/z 355.05 14.40 14.60 14.80 15.00 15.20 48.17% Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 |................... ............................. 5000- 14.40 14.60 14.80 15.00 15.20 m/z 267.00 47.35% 251 323339 | 191207 i ■ " ■ i' " 11 ■ 1 । I । 1 ' । | । | ■T। ■ ■ ■ ■ I I 1 11 ‘1′17711 ( । । ।। । i1''' r 1' n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73

14.40 14.60 14.80 15.00 15.20 5000 355 m/ z 356.05 17.18%

LL 44

m/z-> 40 1881I‘0‘11‘130147 1 193 267 294 ——1r7mm71"B0100Tm51"O ——CT"TT" 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 m Abundance #73975: Benzoic acid, 2,4-bis{(trimethylsilyl)oxy]-, trimet - 73 14.40 14.60 14.80 15.00 15.20 m/z 2 68.00 12.63%

5000 355 45 133j49 ’' i n 111 i1 ■111' * ■11 193 223 i " ‘' i1''11" " i " " I1' " i 281 -PP ....... ' i 1370 '1 r T 1' ’11 " " i I ' 1 ' ' I ' 1 \......... 1 1 1 । 1 ‘ ' r i 1 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

8435.D GCMS0412.M Wed Apr 17 09:48:14 2002 Page 2

NYC-WTC_000048569