GCMS analysis results for sample AE05852, April 23, 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR12O2\5852 .D vial: 7 Acq On : 15 Apr 2002 1:57 pm Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 14.83 2.07 ug/1 368151 Naphthalene-d8 15.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38 3 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 4 Noradrenaline, tetra -TMS 457 C20H43NO3Si4 000000-00-0 37 Abundance J Scan 1066 (14.829 min): 5852.D (-) m/z 73.00 100.00% 73

5000 267 355 ............ J ......... ............ i ■1 ■1111 ■111 45 14.40 14.60 14.80 15.00 15.20 i । ■ ‘ i1"11" ft1 1 89 r, 1 p108 133 154 »17 Pieipu r A * r177193 223 251 r*| TPpr “1. r’H 1 wguarpudni) 293 323339 I —ptmmm m/z 267.00 45.67% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 i ■ ' ■ ■ i • ■ ■ i ■ ■ 14.40 14.60 14.80 15.00 15.20 m/z 355.05 45.51%I 191207 251 323339 TIun ■ i1 “• i““i“■ • i"i ■ “■ i“■ ■ i•■ ■■ i■1 “i■■ ■ ■ i ■ r“I““i•1 ■ ■ i1 ■■ ■ i" i “ ■ ■ i mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy}, trimet 73 1| 14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 16.10% 45

133149 193 223 281 . T’10mu0umuu—uuuunmmumuT[ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy!s i ■ ‘ ■ i ■ ‘ ■ * i • ■ i • 73 14.40 14.60 14.80 15.00 15.20 m/z 268.00 11.81 5000 355 44 , . 130147 193 267 294 | I 1 . . fl, . ] . . ,"r l . 1 . . | .. . . || , I . , . , I . . . , I, . ,, J,, , ,! .. I I. , | I I , . | , i . 111 11 C'l 1 I I I I -nlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

5852.D GCMS0412.M Tue Apr 16 15:40:35 2002 Page 2

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