Gas chromatography-mass spectrometry analysis results for sample AE07115 including detection of unknown compounds.
NYC-WTC_000049063–000049101Folder label: “GCMS X 4/12/02 A 4/23/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR2202\7115.D Vial: 21 Acq On : 23 Apr 2002 4:39 am Operator: Sample : re-ext Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.
14.81 0.43 ug/1 77180 Naphthalene-d8 15.84
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopent as i lox; e, decamethyl- 370 C10H3005Si5 000541-02-6 2 Benzoic acid, 2/,4-bis[(trimethylsil 370 C16H3004Si3 010586-16-0 38 3 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3S13 010538-85-9 38 4 Noradrenaline, tetra-TMS 457 C20H43NO3S14 000000-00-0 37 Abundance ( Scan 1063 (14.806 min): 7115.D () m/ z 73.00 100.00% 73
5000 267 355
45 14.40 14.60 14.80 15.00 15.20 “11 * , . 108 133 154, 177193 . 223 —— T12110-5111/121112111102022012*h 2511.... mRR mT"r 323339 m/z 355.05 41.46% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 ...................... ...................... 5000 14.40 14.60 14.80 15.00 15.20 m/z 267.00 40.20% 191207 251 t 323339 I “ ‘' I ‘ ' i M ' I T‘*mm—2—onm0*02**0T TnT I“"i mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy}-, trimet 73 ......... . 14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 14.98% 45 223 133149 281 193 I 370 ‘ 1121101111011511111111010"3303B91‘3TT0- ■ । । t ■r■" i■i■■" i ■"r i • ■ • ■ i L
mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-. beta.,3,4-tris(trimethyls 73 14.40 14.60 14.80 15.00 15.20 m/z 268.00 11.11% 5000 355 44 It l 88.... 130147 .... 193............ ...................... .... m/z—> 40 60 80 100 120 140 160 180 ‘260' 220 240 260 280 300 '320' '340' 360 ' TI ■ ' i ‘ 14.40 14.60 14.80 15.00 15.20 ' i ■ ■
7115.D GCMS0412.M Tue Apr 23 14:23:04 2002 Page 2
NYC-WTC_000049072
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Laboratory report listing GCMS analysis of surrogates for sample AE07115 on April 15, 2002.
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1 shared topics · similarity 0.986
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1 shared topics · similarity 0.986
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Laboratory report documenting GCMS analysis of sample AE07382 for unknown compounds and surrogates conducted on April 25, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010585
Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.984
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010610
Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.983
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023023
Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09571 conducted on May 14, 2002.
1 shared topics · similarity 0.983
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Laboratory analysis report for sample AE02334 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.983
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1 shared topics · similarity 0.983
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