GC/MS analysis results, sample AE08934, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0302\8934.D Vial: 8 Acq On 3 May 2002 8:54 pm Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.80 2.46 ug/1 197104 Naphthalene-d8 15.82

Hit# of 5 Tentative ID MW MolForm CAS# Qual 77) 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6/9 2 Benzeneethanan ine, N- (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 47 3 Benzoic acid/ 2,4-bis (trimethylsil 370 C16H30O4Si3 010586-16-0 38 4 Noradrenaline, tetra-TMS_________ 457 C20H43NO3Si4 000000-00-0 38 Abundance , Scan 1065 (14.796 min): 8934.D (-) m/ z 73.10 100.00% 73

5000 267 355 ........ I | । > । i | l /.......... i i | I r i I I i I i | i ' i |

45 14.40 14.60 14.80 15.00 15.20 - 108 ।' । 154 193223 323 ■ ■ । ■ । । । 1 I । । ‘ m । । । i । । i > TI——HTTT m/z 355.10 33.66% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 267.05 33.20% ' i ' 1 ' 1 i ■ ■ 1 1 207 i ■ ' 1 ■ 1 ' 323, 1 1 ■ i 1 m/z—>50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 .... .. ■ i ' ’ 1 1 i 1 ' 1 1 i ' 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.10 11.56%

45 208 251 281 386 1 r 1“' 1 1 ''I ' 1 1 ’1 | 1 1 ————————I- TI—dnnn —458 —m—m———548 T m/z-> 50 100 150 200 250 300 350 400 450 500 550 ....... .. ...... .. Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet 73 14.40 14.60 14.80 15.00 15.20 m/z 268.05 8.98% 5000 355 45 133 1 93 223 281 7 — i r t i । i i r i 1 i i i r । + I । i । i 1 - rq i i i i pi i i i । i i i i । i i i i t i i i i ' i r ____________ ___ 1 i 1 ‘ 1 ' I 1 ' 1 1 i 1 1 1 1 i 1 ■ 1 1 i 1 ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

8934.D GCMS0501.M Mon May 06 10:49:04 2002 Page 2

NYC-WTC_000043724