NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\MAY0302\8838.D Vial: 7
Acq On 3 May 2002 7:55 pm Operator:
Sample RE-EXT. Inst : 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
14.79 3.21 ug/1 260765 Naphthalene-d8 15.83
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64
2 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38
3 3,4 -Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 38
4 Benzoic acid. 4-[(trimethylsilyl)ox 282 C13H2203Si2 002078-13-9 37
Abundance / Scan 1064 (14.793 min): 8838.D (-) m/ z 73.10 100.00%
73
5000
267 355
। । । i i y i r-1 । I iiii r" i" |- । ■" |'"i”r
45 14.40 14.60 14.80 15.00 15.20
125 154 193 223 323 I
, 1 I J T । । । । । ।1 r । 'i i'1 । ' । r : । 1 ii i i । i k I | i i LI [“I I I I ] I I I I | l I I | I T m/z 267.05 30.33%
m/z->50 100 150 200 250 300 350 400 450 500 550
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267 । [ i i । i [ r “i i r — i i i । i | i i । i r
5000
14.40 14.60 14.80 15.00 15.20
m/z 355.10 28.09%
— 1*
207 323 1
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene]
73 355
■ । 1 ' 1 1 । '1 ■' i'1 ■' । 1 1 1 ■ । ‘
14.40 14,60 14.80 15.00 15.20
5000 m/z 356.10 10.58%
45
|
। । I ■
|
■ ' । । ■ ■
208■ ' 251
■ । i ■ • ■ ■ । ■ / ■ '
281
f - i ■ ■
386 458 548
‘ 1 i ' 1 1
' i ' 1 ' 1 i ' ■ ' ' i ' ‘ ‘ ■ 'i ' ■
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)-
73 14.40 14.60 14.80 15.00 15.20
m/z 74.10 8.56%
267
5000 179
356
45 147
— 209 237, 312 JI I \ Ul I I I I ■ I I I I I
1II**’IIII*t1um 1 ; i ' ' 1 1 i 1 ' 1 ' 1 1 ' ' ' i ' 1 1 ' i ' ' I I I I I I I I I r
m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20
8838.D GCMS0501.M Mon May 06 10:48:42 2002 Page 3
NYC-WTC_000043676
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