GCMS calibration results for sample AE09580, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\MAY0302\9580.D Vial: 10 Acq On 3 May 2002 10:51 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.79 2.00 ug/1 173818 Naphthalene-d8 15.83 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C10H3005Si5 C16H3203Si3 000541-02- 068595-79-9 47 780 3 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 43 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 Abundance Scan 1064 (14.792 min): 9580.D (-) m/z 73.10 100.00%

5000 267 355 ....... /......... l | i I I I [ I- I— I I | T I T i । i I i i । i ।

45 14.40 14.60 14.80 15.00 15.20 i , |, 108 133 154170 191207223 251 | 323339 L I 1 ' 11 |‘‘‘II‘‘‘‘‘**‘1‘11* 1’’ i[ ITT’, ■ ■ । ■ । । । । i' । । " i । i 'h i [ i' ■ ■ ■ i TTTTTT m/ z 2 67.05 28.85% m/z->______ 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 i । i i i । । । । i r ।y i i i -1 i i i । i r 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 26.20% 191207 251 1 323339 | i ■11111 ■'1 r 11111 ■111 mapamort m/z->______ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 i1 ■111'1'11 i1 * 11 ri 11

Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 ' i 1 ■ ■ 1 i ' 14.40 14.60 14.80 15.00 15.20 +........ 267 m/z 356.10 9.90% 5000 179 356 45 147 I , — 209 237 , | 312 341 I 11" ■' i"11 r11 IIt < i | Il r r | i i r i | r i i i । r i r । | i I । i | i i i i | I 117" I । i r f I | i i r | I 'I |'IT i i

n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #72298: Benzoic acid, 2-[(trimethylsilyl)oxyJ-, trimethylsi .......... V.......... i । ii i i । i i i I । 1 i m । । i i i । । । 73 267 14.40 14.60 14.80 15.00 15.20 m/ Z 74.10 8.07% 5000

47 । 135,175 193209 233249 1 282 TTTUmuu | I । | । I t r । i i i ) '[ । i i i । i i i i । i I i । । | r | | | |" T I I । i i I i | I i i i j i t i i |i i i i । i r 1 1 1 1 - m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

9580.D GCMS0501.M Mon May 06 10:50:14 2002 Page 2

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