GCMS analysis results for sample AE06449, April 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\6449.D Vial: 7 Acq On : 17 Apr 2002 2:06 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 14.81 1.29 ug/1 210324 Naphthalene-d8 15.84 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 68 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 49 3 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 4 Benzoic acid, 2,/4-bis [ (trimethylsil 370 C16H30O4Si3 010586-16-0 38 Abundance ican 1063 (14.807 min): 6449.D (-) m/z 73700 100.00% 73

5000 267 355 | I I I I I I I 1 ‘ I 11 TII 1 1 1 11 1 1 45 14.40 14.60 14.80 15.00 15.20 | 108 133 154 177 193208223 251 j 293 323339 » i ~| r i i । । । । i i । । । । । । TTI———TmmOmur -Hr i1'1' i111111111 TT T ।1 j' 1 m/z 267.00 42.62% mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 -................. — 5000 14.40 14.60 14.80 15.00 15.20 m/ z 355.05 39.75%

i ‘■ i 111'1 i 191207 i1'1 11'1 11 i 251 1 l’1 1111 '11 TTUROgn 323339 mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsiiyl)- 73

14.40 14.60 14.80 15.00 15.20 5000 267 m/ z 356.05 15 .48% 179 356 45 147 1 ■ i ' 1 ' 1 'i 1 ..................... |......... I,,, 1 I 209 237 , 1, 312 341 L ' " r 1 ' " 1 ‘ 1 1 ' I 1 " ' ' J: >' ' 1 1 1 1 " I 1 1 1 1 1' 1 1 I’ i11111"1111111111" i"1 '1'11 T mz— > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls I 1 1 1 ' I ' ' TIT 11 ‘ I I I I I I I 73 14.40 14.60 14.80 15.00 15.20 m/ z 2 68.00 11.57% 5000 355 44 I , 88 130147 193 267 294 | 111 1 1 ‘ i 1 ' 11 I ' 1 ‘ ' I 1 1 ‘ 1 I ' TT । | । । । | । i r । | । i । । | । । । i | > i । । । i ‘i i 11 i i i'i । i i i i । । । । । । i । T । । m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

6449.D GCMS0412.M Thu Apr 18 09:10:45 2002 Page 3

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