NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 20 pages
GCMS analysis results for sample AE02575, March 2002
Machine-extracted title · confidence 90%Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
NYC-WTC_000038871–000038890Folder label: “GCMS X 3/4/02 A 3/20/02”
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NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\MAR1902\2575.D Vial: 24 Acq On : 21 Mar 2002 3:41 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\l\METHODS\GCMS03O8.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
14.86 1.12 ug/1 222178 Naphthalene-d8 15.91
Hit# of 5 ; Tentative ID MW MolForm CAS# Qual ----------------------- j----------------------------------------
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 87 2 Phenethylahine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 3 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38 4 N--(Trifludroacetyl) -N,O,O' Scan 1069 (-) 553 C22H42F3NO4Si4 1 -tetr ,0'2575.D (14.863 min): 000000-00-0 38 Abundance ■ m/z 73.0,0 100.00%
5000 267 355
45 I, 108 125 154 177 193208223 251 |l 293 323339 1 14.60 14.80 15.00 15.20 ' ' I ' I ' ' ' ' TTTITTTTTnur |"' TT TT I IT I | T I I | ‘I I I - i11 " i11 " i " " i'1 " 11111 111 " I m/z 267.00 43.88% m/z-2 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 5000 267 .............. I \......... T ' 1 1 1 ' ' I ' 1 ' I 1 ' ' • I 1 1 14.60 14.80 15.00 15.20 m/ z 355.05 40.43% 191207 251 1 323339 '1 r 1'' i1 ""IT111111111 111 >> 111111 v 11111! 13! 111111 j 1111 ] 1111 11 j t! 111111 ji 111 ] 11 T*1'11 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280300 320 340 360 Abundance 73 —.......... - 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 15.17% 44 88 130 147 193 267 294 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ''' Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet _.................. 1 ' i ' ' ' 1 1 1 1 ' 1 1 1 1 73 14.60 14.80 15.00 15.20 I m/z 268.00 11.58% 5000 355 45
133 149 193 223 281 340 11 370 - r-q-rTT-rp- ‘ । ‘ ‘ । 1 ' 1 1 I । 1 ' ' I 1 ' ' ' I ' ' ' ' | ' I । | ' i' ' । | I . . . | . I I I | I 'l I I |LI I I I | I ! I I | ! I I > ] , I ! T | I I ‘II m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20 |
2575.D GCMS0308.M Thu Mar 21 14:23:27 2002 Page 2
NYC-WTC_000038879
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