NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\MAR2502\LB.D Vial: 9
Acq On : 25 Mar 2002 6:05 pm Operator:
Sample : gc/ms scan 2/28 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
14.85 1.41 ug/1 273291 Naphthalene-d8 15.88
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 68
2 Phenethylai ine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38
3 Benzoic ad d, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 38
4 N- (Triflubroacetyl)-N,O,O',0' 1-tetr 553 C22H42F3NO4Si4 000000-00-0 38
Abundance $ Scan 1068 (14.847 min): LB.D (-) m/z 73.00 “100.00%
73
5000 267 355 -
45 , i 103118133 154 177193 223 251 j 293 323339 [ 14.60 14.80 15.00 15.20
■■ i"i j ****jaa*Vds i | f I | . ii [% i • ’l 1 Ji 1’* ***** .] . ’Ta | it. i I ‘ ‘ I* r. । \ . । | . . । Fj m/z 267.0 45.02%
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355 --
267
5000
14.60 14.80 15.00 15.20
m/z 355.05 43.73%
, . 191207 2?1 j 323339 |
TTITTmImm‘umm/umum“m‘uu0—nh‘n—Tu‘1"h3 ‘ t ■ • ■ ‘ i “ “ i * ■ ■" i" “ i
m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance 4 /_ C 5
73
14.60 14.80 15.00 15.20
5000 355 m/z 356.0 15.38%
44
; 88 130 147 193 267 294
miz-s____ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance" #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet
73 355 14.60 14.80 15.00 15.20
m/z 268.00 12.18%
5000
147 267
249
47
TTp-rTTpnn-rpnnTpnTnyrTTTp-TTTpT^^
208
Itr 28: • ■ i ■■ ■■ 11■ j1' '“1 i370
1 ■■■11
14.60 14.80 15.00 15.20 |
m/z~> 4060 80 100 120 140 160 180 200 220 2401 260 280, 300 320 340 360
LB.D GCMS0308.M Thu Mar 28 12:38:38 2002 Page 1
NYC-WTC_000011843
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