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GCMS blank analysis results for sample AE04388, March 2002

Machine-extracted title · confidence 100%

Laboratory report of a GCMS blank run for sample AE04388 conducted on March 28, 2002.

NYC-WTC_000011837–000011844

Folder label: “GCMS X 2/28/02 A 3/26/02

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Scanned page image, NYC-WTC_000011843
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2502\LB.D Vial: 9 Acq On : 25 Mar 2002 6:05 pm Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.85 1.41 ug/1 273291 Naphthalene-d8 15.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 68 2 Phenethylai ine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 3 Benzoic ad d, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 38 4 N- (Triflubroacetyl)-N,O,O',0' 1-tetr 553 C22H42F3NO4Si4 000000-00-0 38 Abundance $ Scan 1068 (14.847 min): LB.D (-) m/z 73.00 “100.00% 73

5000 267 355 -

45 , i 103118133 154 177193 223 251 j 293 323339 [ 14.60 14.80 15.00 15.20 ■■ i"i j ****jaa*Vds i | f I | . ii [% i • ’l 1 Ji 1’* ***** .] . ’Ta | it. i I ‘ ‘ I* r. । \ . । | . . । Fj m/z 267.0 45.02% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 -- 267 5000 14.60 14.80 15.00 15.20 m/z 355.05 43.73% , . 191207 2?1 j 323339 | TTITTmImm‘umm/umum“m‘uu0—nh‘n—Tu‘1"h3 ‘ t ■ • ■ ‘ i “ “ i * ■ ■" i" “ i m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance 4 /_ C 5 73

14.60 14.80 15.00 15.20 5000 355 m/z 356.0 15.38% 44 ; 88 130 147 193 267 294 miz-s____ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance" #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet 73 355 14.60 14.80 15.00 15.20 m/z 268.00 12.18% 5000

147 267 249 47 TTp-rTTpnn-rpnnTpnTnyrTTTp-TTTpT^^ 208 Itr 28: • ■ i ■■ ■■ 11■ j1' '“1 i370 1 ■■■11 14.60 14.80 15.00 15.20 | m/z~> 4060 80 100 120 140 160 180 200 220 2401 260 280, 300 320 340 360

LB.D GCMS0308.M Thu Mar 28 12:38:38 2002 Page 1

NYC-WTC_000011843

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NYC-WTC_000011843Source: NYC Law Department, mirrored locally

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