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GCMS analysis results for sample AE06637, April 2002

Machine-extracted title · confidence 100%

DEP laboratory report of GCMS analysis for sample AE06637 conducted on April 18, 2002.

NYC-WTC_000060504–000060512

Folder label: “GCMS X 3/21/02 A 4/16/02

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Scanned page image, NYC-WTC_000060511
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1602\6637.D Vial: 10 Acq On : 16 Apr 2002 10:01 pm Operator: Sample : gc/ms scan 3/22 fb Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 14.81 1.91 ug/1 358836 Naphthalene-d8 15.85 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopenta loxane, decamethyl- 370 C10H3005Si5 000541-02-6 68 2 Benzoic ao d, 2,6-bis [ (trimethylsil 370 C16H30O4Si3 003782-85-2 38 3 N-(Triflub roacetyl)-N,O,O',0''-tetr 553 C22H42F3NO4Si4 000000-00-0 38 4 Pheneth; amine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 <\bundance Scan 1064 (14.809 min): 6637. D (-) m/z 73.00 100.00% 73

5000 267 355

45 14.40 14.60 14.80 15.00 15.20 I I 100125 1^ 193 223 ,, 293 323' 1 , , , .......... ''' I ' ''''' I ” I''' '■ 'r'' m/z 355.05 45.79% n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 / V ■ 5000 14.40 14.60 14.80 15.00 15.20 m/ 2 267.00 45.66% 323,...................................................... m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet 73 355

14.40 14.60 14.80 15.00 15.20 223 m/z 356.05 16.48% 147 267 47 208 237 J Ti/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi ■p^ 73 14 40 14,60 14.80 15.00 15.20 m/z 268.00 12.12% 355 553

45 I 50 h 100 147 *150 193 200 250 267 300 350 400 450 500 538 550 l\ 14.40 14.60 14.80 15.00 15.20

6637.D GCMS0412.M Wed Apr 17 12:03:36 2002 Page 1

‘ NYC-WTC200b06b51 i '

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NYC-WTC_000060511Source: NYC Law Department, mirrored locally

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