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GCMS analysis results, sample AE05236, April 2002

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Laboratory report documenting GCMS analysis of sample AE05236 for unknown compounds on April 9, 2002.

NYC-WTC_000059185–000059195

Folder label: “GCMS X 3/9/02 A 3/30/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5236.D Vial: 47 Acq On : 31 Mar 2002 2:36 pm Operator: Sample : gc/ms scan 3/9 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.85 0.28 ug/1 44582 Naphthalene-d8 15.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopenta^loxane, decamethyl- . 370 C10H3005Si5 000541-02-6 59 2 Phenethylarhine, N-methyl- .beta. , 3,4 399 C18H37NO3Si3 010538-85-9 38 3 N-(Trifluc/toacetyl) -0,0',0' '-tris (t 481 C19H34F3NO4Si3 000000-00-0 38 _4_N2.(Tr£flriproacetyl)-N, 0,0','O' '-tetr 553 C22H42F3NO4S14 000000-00-0 38 Abundance / Scan 1068 (14.847 min): 52~36.D (-) m/z* 73.00 100.00% 713

5000 355 267 i 45 133154 193 , 323 I 14.60 14.80 15.00 15.20 ! ' I ' ' ' l' ■ ' ' 7 I ' ' ' ' I ' ' I ' ' ' ' ( ' ' ' ' I ' m/z 355.05 48.33% ___ 50 100 150 200 250 300 350 400 450 'Abundance #51266: Cyclopentasiloxane, decamethyi- 713

5000 267 355 ... n..... 14.60 14.80 15.00 15.20 I m/z 267.00 41.36% I 207 323 ,................................. 'm/z~> 50 100 150 200 250 300 350 400 450 Abundance #74239: Plionethylamine, N-irietliyl-.beta,,3,4-tris(tr!iTietbyls 713 ...... 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 14.78% 44 I 147 193.... ........... 1 I ' ' I 50 100 150 200. 250 300 350 400 450 'Abundance #58326; N-(Trifluoroacetyl)-b,d',d"-tris(trimethylsilyr)no 713 14.60 14.80 15.00 15.20 355 m/z 357.05 10.73% 5000

45 I I 126147 193 265 376 481 I , 50 100 150 200 250 300 350 400 450 14J014;80 15.00 15.20

5236.D • GCMS0308.M Wed Apr 03 14:02:36 2002 Page 3

NYC-WTC_000059194

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NYC-WTC_000059194Source: NYC Law Department, mirrored locally

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