GCMS analysis results, sample AE05236, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5236.D Vial: 47 Acq On : 31 Mar 2002 2:36 pm Operator: Sample : gc/ms scan 3/9 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title :' 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4^hydroxy-4-methy Concentration Rank 2

R-.T. EstConc Area Relative to ISTD R.T.

8.24 0.29 ug/1 36870 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone,/4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 45 2 2-Propanone,/ 1-cyclopropyl- 98 C6H10O 004160-75-2 9 3 5-Hexen-2-ohe 98 C6H10O 000109-49-9 9 4 1,3-Dioxan®, 4,4-dimethyl- 116 C6H12O2 000766-15-4 9 Abundance 7 413 m/z 4377)0.. ioo7oo% 59 5000

101 , A, I ! Tr".p^.|l4tn.i| 7.80 8.00 8.20 8.40 8.60 I'' I' I" " I''" I" 1' I I " '' I m/z 59.0,5 ‘ ■ 58.42% 'n)/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- I 43

5000 , , , I-, , A \o|7S,, I , , , 7.80 8.00 8.20 8.40 8.60 m/z 100.95 22.46% 27 101 I ‘' I' I ’' J "' I" " I' I 8.3 I" " I"'' I “ ‘' I I'"' J "' I" " I m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1306: 2-Prepanone. 1 -cyclopropyi- 43

7,80 8.00 8.20 8.40 8.60 5000 m/z 58.0,5 17.01% 55 29 83 98 69 jrrrrp 7" " I m/z->5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63205:5-Hexen-2-one 43 7.80 .8.00^4,1 ,..... 8.20 8.40 8.60 m/z 39,.05 10.48% 5000

27 55 15 50 83 98 I" I' I “ " I" " I" I' I 'm/z--> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 7.80 8.00 8:20 8.40 8.60 [

5236.D GCMS0308.M Wed Apr 03 14:02:32 2002 Page 2

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