GCMS sample AE05062 analysis, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\M7kR3 0 02\5056.D Vial: 32 Acq On : 30 Mar 2002 11:42 pm Operator: Sample : gc/ms scan 3/8 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.24 0.32 ug/1 40408 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanon^, 4-hydroxy-4-methyl - 116 C6H12O2 . 000123-42-2 50 2 Acetone / 58 C3H6O 000067-64-1 9 3 5-Hexen-^-one 98 C6H10O 000109-49-9 9 4 2-Propione, 1-cyclopropyl- 98 C6H10O _2.2416O-_75-_2 ■ ........... 9 Abundance t Scan 348 {8T239 mTn): 5O56’D (-f ' 43

5000 59

101 83 7.80 8.00 82P 8.40 8.60 ■........ i|'l 51 I ‘ ' I ' ' ' ' I ‘ ' I 4-/'■' ' ' I m/ z 48.96% 'm/z-> 10 20 . 30 40 60 70 80 90 100 Abundance #3245; 2-Pentanone, 4-hydroxy-4-methyi- i 4b

5000 59 7.80 8.00 8.20 8.40 8.60 101 m/z 100.95 24.48% 31 H i 73 S3 A I 1

10 20 30 40 50 60 70 80 90 100 Abundance #94: Acetone 43 A 7.80 8.00 8.20__ 8,^ 8.60 5000 m/ z 57.95 17.42% 15 58 27 I ' ' ‘ ' I ' ' ‘ ' I ' ' ' ' I ' ’ ' ’ I ' ‘ ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' T rn/z-> 10_ JO _ 30 40 50 60 70_ 80 90 100 Abundance ■# 1291: 55iffi!^2^.... -r——r-> 43 7.80 8.00 8.20 8.40 8.60 m/z 41.95 7.53% 5000

55 ,.,..,.7,..37 50 I 69 83 98 10 20. 30 40 50 60 70 80 90 100 7.80 8.60

5056.D GCMS0308.M Tue Apr 02 15:34:05 2002 Page 2

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