GCMS calibration table data, sample AE09682, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY0602\9682.D Vial: 25 Acq On : 7 May 2002 3:49 pm Operator: Sample : GC/MS SCAN 4/25 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.16 11.36 ug/1 919310 1,4-Dichlorobenzene-d4 12.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9 3 5-Hexen-2-one 98 C6H10O 000109-49-9 7 4 Acetone 58 C3H60 000067-64-1 7 Abundance Scan 340 (8.156 min): 9682.D (-) m/z 43.05 100.00% 43

5000 59

7,80 8.00 8.20 8.40 8.60 101

m/z-> ........................... ' ■ l1 ' 10 38 1 1 I 1 1 1 ‘ I 1 ■ 11 I 1 20 30 40 +53+ 50 I. .,6?...... . .......... ............ m/z 59.10 60 70 42.64% ‘ I ■ ■ • ■ i • ■ ■ • i ■ ■ 1 ■ i 1 ■ 1 ' r' 1 1 ' i 1 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 8.60 m/z 58.10 16.52% 27 101

niz—> 10 20 I I 30 H 40 +4950—+ 60 70 i ‘ 80 ■ i ■ ■ ■ ■ i 83 । ‘ i ■ ‘ ■ 1 i ■ ■ ■ ■ i 90 100 110 ■

Abundance #1448: CH2=CHCH2C(O)OCH3 43 7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.56%

34,4 72 —T100 miz-s 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205: 5-Hexen-2-one 43 7.80 8.00 8.20 8.40 8.60 m/z 41.05 7.00% 5000

27 55 15 50 83 98 miz—> 1 ■ i ■ ■ ■ ■ i ‘ '■ ■ i 1 1 10 20 30 38+ 40 1 • ■ i *lu ■ i ' ' ■ ' i ■ ' ■ ■ i 50 60 70 80 ' i ■ ■ — 90 100 110 TTm—nm——/mBnnTmur 7.80 8.00 8.20 8.40 8.60

9682.D GCMS0501.M Thu May 09 11:26:12 2002 Page 1

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