GCMS calibration table data, sample AE09682, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0 602\9682.D Vial: 25 Acq On 7 May 2002 3:49 pm Operator: Sample GC/MS SCAN 4/25 Inst ; 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Benzamide, N-propyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

33.34 0.79 ug/1 52031 Chrysene-dl2 33.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzamide, N-propyl- 163 C10H13NO 010546-70-0 37 2 Morpholine, 4-phenyl- 163 C10H13NO 000092-53-5 25 3 1-Benzoyloxy-2- formyl oxybenzene 242 C14H10O4 797922-93-1 16 4 Ethanone, 2- (acetyl oxy) -1 -phenyl - 178 C10H10O3 002243-35-8 12 Abundance Scan 3088 (33.338 min): 9682.D (-) m/z 105.05 100.00% 105

5000 149 163 77 T4 51 33.00 33.20 33.40 33.60 41_ ■ ■ i", ■ ' ‘ i ■ • • ■ i 207 ■; 1 ■ i ■ ■ ■ i ' ■ ’ 1 i ■ ■ • ■ i ■ ■ ■ • i ■ ■ • ■ i ■ 1 1 1 I 1 ' m/z 149.05 40.39% nz-> 40 60 80 100 120 140 160 180 200 220 240 __ Abundance #13165: Benzamide, N-propyl- 105

5000 77 33.00 33.20 33.40 33.60

A 163 m/z 163.15 40.30% 51

niz-> 40 iadijam 60 80 ........... 1 I ‘ k ‘ ' I ‘ 100 120 122 134 148 , ‘ l‘ 1 1 * I • 1 k 1 I 1 ‘ ‘ ’ I ’ ’ 140 160 180 * I ‘ ' 1 ‘ 1 1 * 1 1 I 1 1 200 220 240 Abundance #13173: Morpholine, 4-pheny- 105 ' '1' 1 11 I' 1 1 1 I ' ’ ■ 33.00 33.20 33.40 33.60 5000 m/z 77.10 35.85% 77 163

AM 51 91 132 — TIB————T ■117 ■ i ■ • 1 • i ■ ■ ■ ■ i 1 ■ ■ ■ i ■ 1 r ■. i 1 1 1 1 1 1 1 ' 1 1 1 ' miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #32316:1-Benzoyloxy-2-formyloxybenzene T I 1 1 1 ‘ 1 1 ’ r1 I r ‘ l k 105 33.00 33.20 33.40 33.60 m/z 51.10 10.31% 5000 77

51

m/z—> kJ. .,?.. I,., 40 60 80 >■ -J, . > 100 120 140 160 180 197 200 214 220 242 240 ■ ■ I • • 33.00 33.20 33.40 33.60

9682.D GCMS0501.M Thu May 09 11:26:13 2002 Page 2

NYC-WTC_000013283