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GCMS analysis results for sample AE05745, April 11 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE05745 conducted on April 11, 2002, including surrogate recovery data.

NYC-WTC_000059555–000059564

Folder label: “GCMS X 3/12/02 A 4/2/02

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Scanned page image, NYC-WTC_000059562
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0102\5746.D Vial: 25 Acq On 3 Apr 2002 12:59 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.14 1.94 ug/1 270213 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethyl mrmamide 73 C3H7NO 000627-45-2 9 2 1,3-Dio/olane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 3 3-Pent^ol, 3-methyl- 102 C6H14O 000077-74-7 9 4 Acetamide, N-methyl- 73 C3H7NO 000079-16-3 7 Abundance ’ Scan 337 (8.136 min): 5746.0 (-) “mTz. 73Tm 100.00% 70

5000 43 ...................... 87 7.80 8.00 _82^ 8,40____ I I ' I I , ' , I ' ' ' ' I , I I ‘' 111 I 49 55 , I I 103 ' ' I ' ' ‘‘‘‘l ' m/z 43.05 25.“3 7% m/z-> JO 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethyiformamide 3|0 73 ! i 5000 44 58 7.80 8.00 8.20 8.40 m/z 41. Q5 9.74% ^.5 J J. , ' I ' ‘ ' ' I ' ' ' ' I ' ' ' ' I ' 'm/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolaria. 2-(3-brorrio-5,5,5-tricbioro-2,2-diiTie! 7'3

__ 7.80 8.00 8.20_ 8.40 5000 m/z 45.05 9.11% 45 36 55 67 109 115 I 'm/2-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #63573: 3-Pentanol, 3-methyl- 7f3 7.80 8.00 8.20 8.40 m/z 71.00 7.31% 5000 55 87 y , 39, I ^,-,^,1, ,l|... J........... m/2-> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40

5746.D GCMS0403.M Fri Apr 05 10:38:35 2002 Page 1

NYC-WTC_000059562

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NYC-WTC_000059562Source: NYC Law Department, mirrored locally

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