GCMS analysis results for sample AE04730, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\M71R2602\4730.D Vial: 12 Acq On : 26 Mar 2002 8:36 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library :. C:\DATABASE\NBS75K.L ★★********************************************************* ********** Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.14 2.04 ug/1 300912 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethyl/ormamide 73 C3H7NO 000627-45-2 9 2 Silane/ tetramethyl- 88 C4H12Si 000075-76-3 9 3 3-Pentanol, 3-methyl- 102 C6H14O 000077-74-7 9 4 Ethylamine 45 C2H7N 000075-04-7 4 ■Abundance Scan 33^(87136 min); 473b.b m/z..... 73Tm.. ... lOOT^ 7(3

5000 43 T-T—f—I—r—r-T—p

S? 103 7.80 8.00 8.20 8.40___ ....................................... 3,Q,l, I 50 55 , , r-r-rA-q— m/ z 43.05 28.80% m/z-> 10 20 30 40 ..... ,50........ .60.,....... 70 80 90 100 110

L Abundance #292: N-Ethylformamide 3b 73

5000 58 7.80 8.00 8.20 ^0______ 44 m/z 10.98% +-n- m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845. Silane, tstrarnethyi- 73 .......... ; ....................... 7.80 8.00 8.20__ 8,40______ 5000 m/z 41.05 10.15%

45 15 31 ,1 55 '.................................. 86............................. ■ ni/z-> 10 20 30 ■ 40 ' ' 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol. 3-methyl- 7|3 7.80 8.00 8.20 8.40 m/z 71.00 6.92% 5000 55 45 87 27 I , 39, I I ' I ‘ ' I I in/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 .8.40

4730.D GCMS0308.M Thu Mar 28 16:31:45 2002 Page 1

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