GCMS analysis results for sample AE07503, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1802\7503.D Vial: 11 1 Acq On : 20 Apr 2002 3:21 am Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.11 0.30 ug/1 36848 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethy ormamide 73 C3H7NO 000627-45-2 9 2 Penta , 3-methoxy- 102 C6H140 036839-67-5 4 3 3-Pe tanol, 3-methyl- 102 C6H140 000077-74-7 4 4 Sil e, tetramethyl- 88 C4H12Si 000075-76-3 4 Abundance Scan 334 (8.110 min): 7503.D (-) m/ z 73.00 100.00% 73

5000 43 | i | | > i I | | i 1 m i | I r i i | I

7.80 8.00 8.20 8.40 i । । i i । । । i । । । [ r ,1,1 1 , 51 59 । I , ) 87 103 m/z 43.05 32.16% 1 1 ■ i 1 1 1 ■ i ■ 1 1 ‘i 1 ‘it i i r | i I r | i r i i Ti * i i l | r

rn/z-> 10 20 30 40 50 70 60 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

5000 7.80 — h. A. 58 8.00 8.20 8.40 44 m/ z 41.05 11.59% 15 > ■ i ■ •1 • > । । I ----- > I i I i r [ i I ” i ~ i | -i ” i ” I-> | i i i i | i i i i । i

n/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 70 1 ■ 1 i 1 A— , A A AAA , , ' ' I 11 ' 1 i 1 r 1 1 i 7.80 8.00 8.20 8.40 5000 m/ z 44.95 9.81% 45

I ' ' ■ ■ I ' ' ' ' I ' ' ' ' I ' 27 33 39 55 I ‘ ' I । ■ i ■ ■ । 1 I > > । । । । m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- ” ' ' ' [ ' 1 ' ' I ' ' ' ' I ' 1 ' ' I 1 1 ' ' I 73 7.80 8.00 8.20 8.40 m/z 71.00 7.38%

5000

55 45

m/z—> 10 ,,,,,,,, ,1, 1 20 27

30 391 1 । 1 1 40 ■ i ■ ■ 50 1'1 i 60 —— 70 80 87

90 —— 100 110 1... 7.80 8.00 8.20 8.40

7503.D GCMS0419.M Mon Apr 22 10:44:08 2002 Page 1

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