GCMS analysis results for sample AE06451, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\APR1 702\6451.D Vial: 9 Acq On : 17 Apr 2002 4:03 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 8.10 2.88 ug/1 370006 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylfibrmamide 73 C3H7NO 000627-45-2 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 4 Ether I 74 C4H10O 000060-29-7 4 Abundance Scan 332 (8,096 min): 6451 D (-) m/z 73.00 100.00% 73

5000 43 1 1 ' I ' ' I TI II I I [ 1 I 11[ I I I I 7.80 8.00 8.20 8.40 ....................................... 38 j h 50 55 67 | 87 103 ■ ' i ‘ ■ ■ ■ i ‘ ■ ■ ■ i ■ ' ' ■ | 1 । ' 1 i * > ■ । । । i ।' । ■ i ■ i ——— m/ z 43.00 27.87% mZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 33 73

5000 58 7.80 8.00 8.20 8.40 44 m/z 41.05 9.91%

m/z-> 415 —4 ■ — 10 20 30 40 50 60 i ' ' ' 1 1 ■ 1 ■ ' i 1 1 ' ■ i ■ 1 1 1 1 1 1 1 ' I ' 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73 ' ' ‘ | 1 "[ ’ . । । . < r > !l । । । 7.80 8.00 8.20 8.40 5000 m/ z 45.05 9.14%

45 15 1 53 59 |............. 88................ — ——— mlz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73 7.80 8.00 8.20 8.40 m/z 71.00 6.50% N 5000

55 45 87 27

m/z-> I , । ■ 1 1 ■ i • • • • । । 10 20 30 39,1 ■ i ■ ' • 40 50 .:

60 I

70 |

80 . I

90 100 __ _

110 7 I ] I I J I ] TI I I [ I T I I I F 7.80 8.00 8.20 8.40

6451.D GCMS0412.M Thu Apr 18 09:11:51 2002 Page 1

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