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GCMS analysis results for sample AE06451, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06451 conducted on April 19, 2002, by the DEP.

NYC-WTC_000039535–000039544

Folder label: “GCMS X 3/19/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\6451.D Vial: 9 Acq On : 17 Apr 2002 4:03 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 8.24 0.36 ug/1 46463 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130> 000918-00-3 33 2 1-Octadecanol 270 C18H380 000112-92-5 9 3 Dotriacontane 451 C32H66 000544-85-4 9 4 N-Acet^Lpyrrolidone ______________ 127 C6H9NO2 000932-17-2 7 Abundance T Scan 348 (8.243 min): 6451 .D (-) m/z 42.95 100.00% 43

5000

1! ' t 82 4 03125 111 7.80 8.00 8.20 8.40 8.60 ' ' I 11 1 » 1 ■ ■ i 1 1 ' i ■ 1 , TLl1ft T > . r-T—। ■ -i-r-T—r->—r-T—j—r m/z 124.85 11.72% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

5000 I ,-i-r-r-pr > > i । . 7.80 8.00 8.20 8.40 8.60 m/ z 81.95 9.89% 15 I 85 125 m/z—> 50 100 150 200 250 300 350 400 450 Abundance #72027:1-Octadecanol 43 । 1 1 1 ' । 1 ' ‘ ‘ i ' 1 1 1 i 1 1 1 1 i 1 1 1 7.80 8.00 8.20 8.40 8.60 5000 82 m/z 96.95 9.66%

m/z-> LL‘1 50 100 ' i 1 ‘ ' 1 i ' 150 200 224 270 1 1 i ‘ 1 1 1 I 1 1 11 I 11 1 1 1 1 ' 1 ' I ' 250 300 350 400 450 Abundance #74490: Dotriacontane ..... II...... i 1 1 1 ' i ' 1 1 ■ । ' 1 1 1 i 1 1 1 i 1 1 1 43 7.80 3.00 8.20 8.40 ).60 m/z 82.95 8.80% 71 5000

l i 97 . L II. 1127 155 183 ___________ 379 407 I T T 1 ] Trr r !d T Tt 1 1 1 1 1 1 1 1 [ 1 1 1 1 [ 1 1 1 1 | 1 1—1—1—|—T 450 ----- m/z—> 50 100 150 200 250 300 350 400 450 7 80 3.00 8.20 8.40 8.60

6451.D GCMS0412.M Thu Apr 18 09:11:52 2002 Page 2

NYC-WTC_000039543

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NYC-WTC_000039543Source: NYC Law Department, mirrored locally

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