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GCMS analysis results for sample AE05848, April 17 2002

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Laboratory report documenting GCMS analysis of sample AE05848 conducted on April 17, 2002, including surrogate recovery data.

NYC-WTC_000059629–000059638

Folder label: “GCMS X 3/12/02 A 4/4/02

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Scanned page image, NYC-WTC_000059637
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0402\5849.D • Vial: 23 Acq On 4 Apr 2002 7:47 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 8.27 1.20 ug/1 54089 1,4-Dichlorobenzene-d4 12.25 Hit# of S Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C13OI 000918-00-3 28 2 N-Acenylpyrrolidone 127 C6H9NO2 000932-17-2 10 3 Tridecane 184 C13H28 000629-50-5 9 4 Eicosane 282 C20H42 000112-95-8 9 Abundance Scan 351 (8.270 min): 5849.D (-) m/z 43705 100.00% 43

5000

125 . J 77,.. 8.00 8.20 8.40 8.60 63 82 99 1, m/z 124.95 11.87% Tife-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 'Kbundance #12247: 2-Propanone, 1.1.1 -trichloro- 43

5000 8.00 8.20 8.40 8.60 m/z 42.00 9.59% 15 I 85 97 125 I " " I" '' I'« " I '''' I ‘''' I Tife-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #4732: N-Acetylpyrrolidone 43

8.00 8.20 8.40 8.60 5000 m/z 81785 7738% 99 127 30 56 86 . 112 1''' ‘I'''' I " '' I •n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69019: Tridecane 43 5(7 8.00 8.20 8.40 8.60 m/z 46795 7.20% 71 5000 85

TiZz-> 27 774 J , 113 184 127 I.I.,I... 11.... I.... I.... I. p ''' I' 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 I" " p "' I Limiu 8.00 8,20 8.40 8.60

5849.D GCMS0408.M Tue Apr 16 08:17:38 2002 Page 2

NYC-WTC_000059637

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NYC-WTC_000059637Source: NYC Law Department, mirrored locally

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