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GCMS reference data for sample AE05847, April 16 2002

Machine-extracted title · confidence 90%

Reference data report listing component names and response values for calibration verification conducted on April 16, 2002.

NYC-WTC_000059608–000059618

Folder label: “GCMS X 3/12/02 A 4/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\APR0402\5847 .D Vial: 21 Acq On 4 Apr 2002 5:48 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 8.27 1.00 ug/1 45963 1,4-Dichlorobenzene-d4 12.25 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propane^, 1,1,1 - trichloro- 160 C3H3C13O• 000918-00-3 56 2 Ethanol, /2,2,2-trichloro- 148 C2H3C13O• 000115-20-8 9 3 N-AcetyTpyrrolidone 127 C6H9NO2 000932-17-2 7 4 IH-Azojaine, octahydro- 127 C8H17N 005661-71-2 4 <Kbundance Scan 352 (8.275 min): 5847.D (-) m/z 43700 100.00%

5000

83 97 125 8.00 8.20 8.40 8.60 35 I 61 17 II '' p ''' p I'' p ''' 111 T-p-n-r-p- |l'i'....... I''i -p-T¥-r"p-TVr m/z 124.85 17755% ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 40

5000 ....... 117...... 8.00 8.20 8.40 8.60 m/z 97785 9744% 15 1 : ■''' I' 35 85 97 117 125 ‘t'p-TTTp-T-rT-p-rTTTT-prl^ . 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66531: Ethanol, 2,2,2-trichloro- 31 ........... 8.00 8.20 8.40 8.60 5000 m/z 87775 8731% 49 77 113 ......... ...... Ill,, III, I ' ' ' ' I ' ' ' ' I 150 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #4732: N-Acetylpyrrolidone 40 8.00 8,20 8.40 8.60 m/z 46785 7.55%

5000

99 127

■n/z-> ............ I' 10 20 30

30 40 .

50 56

60 70 80 86 112 90 100 110 120 130 140 150 LI.. n... . 8.00 8 20 8 40 8 60

5847.D GCMS0408.M Tue Apr 16 08:17:10 2002 Page 3

NYC-WTC_000059617

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NYC-WTC_000059617Source: NYC Law Department, mirrored locally

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