Reference data report listing component names and response values for calibration verification conducted on April 16, 2002.
NYC-WTC_000059608–000059618Folder label: “GCMS X 3/12/02 A 4/4/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C: \HPCHEM\l\DATA\APR0402\5847 ..D Vial: 21 Acq On : 4 Apr 2002 5:48 pm Operator: Sample : gc/ms scan 3/12 Inst : GC/MS 209 Mise : Multiplr: 2.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,3-Dioxolane, 2-(3-bromo-5,5, Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T. 8.13 8.01 ug/1 369520 1,4-Dichlorobenzene-d4 12.25 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,3-Dioxo]fene, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 17 2 1,3-Dioxolane, 2-methyl- 88 C4H8O2 000497-26-7 9 3 Silane, tramethyl- 88 C4H12Si 000075-76-3 9 4 N-Ethylf(/rmamide_______ _ ________ 73 C3H7NO 000627-45-2 9 Abundance Scan 336 (8.128 min): 5847.D (-) m/z 73.00 100.00% 70
5000 43 ................ ....................... 87 7.80 8.00 8.20 8.40 37, I, I 49 55 103 I ' I ' ' ' ' I ' ' ‘ >’ I ' ' I < I > m/z 43.00 29.18% m/z-> 10 20 30 40 50 60 TO 80 90 100 110 120 Abundance #49423:1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet 70
552 7.80 8.00 8.20 8.40 45 m/z 45.05 10.65% 3,6 j l 65 67, 109115 ‘ I ' ' ' ' I ‘ ' I ‘ 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62902:1,3-Dioxolane, 2-methyl- 70 7.80 8.00 8.20 8.40 552 43 m/z 41.05 10.11% 58 27 87 ' ' I ' ' ' ' I ' ' ’I'' ' ' ' I I ' ‘ I ' ‘ ' I ' ' ' H ' I ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' m/^-> .10 20 30 . 40 50 60 70 80 90 100 110 120 Abundance #62932: Silane, letramethyl- 70 7.80 8.00 8.20 8.40 m/z 71.00 6791%
_L . 5000
45 15 I 53 59 1 1 . ....... I I I'- ' I ............ I......... 88............................... Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40
5847.D GCMS0408.M Tue Apr 16 08:17:09 2002 Page 2
NYC-WTC_000059616
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NYC-WTC_000059619
Laboratory report documenting GCMS analysis of sample AE05847 conducted on April 17, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059650
Laboratory report documenting GCMS analysis of sample AE05851 conducted on April 17, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059526
Laboratory report documenting GCMS analysis of sample AE05703 conducted on April 11, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059639
Laboratory report documenting GCMS analysis of sample AE05849 conducted on April 17, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059629
Laboratory report documenting GCMS analysis of sample AE05848 conducted on April 17, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059555
Laboratory report documenting GCMS analysis of sample AE05745 conducted on April 11, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059286
Laboratory record of gas chromatography mass spectrometry analysis for unknown compounds and surrogates on April 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059565
Laboratory report documenting GCMS analysis of sample AE05746 conducted on April 11, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059545
Gas chromatography/mass spectrometry analysis of sample AE05745 performed April 11, 2002, with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059267
Laboratory record of gas chromatography mass spectrometry analysis for unknown compounds and surrogates on April 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058627
Instrument data for GCMS method 508 scan including internal standards from March 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011789
Laboratory report documenting GCMS analysis of environmental sample AE04130 conducted on April 1, 2002.
1 shared topics · similarity 0.997
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NYC-WTC_000059585
Administrative record from the Department of Environmental Protection regarding World Trade Center activities in March 2002.
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NYC-WTC_000059586
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Technical record detailing laboratory method parameters including drip rates and reagent volumes for sample processing.
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NYC-WTC_000059599
Laboratory report showing GCMS blank analysis results for sample AE05847 conducted on April 16, 2002, with compound detection limits.
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Calibration report listing detector response values and minimum detection levels for various organic compounds analyzed on April 16, 2002.
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