GCMS analysis results for sample AE00102, Feb 13 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File :■ C:\HPCHEM\1\DATA\JAN2402\102.D Vial: 9 Acq On : 24 Jan 2002 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-(3-bromo-5,5, Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.44 3.59 ug/1 1016180 1,4-Dichlorobenzene-d4 11.49

Hit# of 5 Tentative ID MW MolForm CAS# . Qual

1 1,3-Dioxolne, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 23 2 1,3 -Diox lane, 2-methyl- 88 C4H802 000497-26-7 9 3 N-Ethylf rmamide 73 C3H7NO 000627-45-2 9 4 Silane,/tetramethyl- 88 C4H12Si 000075-76-3 9 Abundance Scan 261 (7.439 min): 102.D (-) m/ z 72.95 100.00% 73

5000 43

7.00 . 7.20 7.40 7.60 7.80 । । i-i i-r| i i37,1, I . . 55, 61 67,1. l • i • • 87 i i । .... । . . . . । ■ •' ■ > 103 m/z 43.0.5 32.64% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet 73

5000- PmPmmmeor 7.00 7.20 7.40 7.60 7.80 45 m/z 45.05 11.80% 36 .1 ! 5.5 67 , 109 115 I n ■ i ■ ■ ' ■ i ' ' 1 ' i ' 1 ■ ' i ■ 1 ' ■ I 1 • ' ■ i ■ ' 1 ' i 1 ■ ■ ■ i ■ ' ■ ■ i '

m/z—> 10 20____ 30 40 50 60 70 80 90 100 110 120 Abundance #62902: 1,3-Dioxolane, 2-methyl- 73 1*** ‘(77s(*** 7.00 7.20 7.40 7.60 7.80 5000 43 m/z 41.05 11.13% 58 27 87 110010111 1 1 s I i miz-> 10 20 30 40 50 60 70 80 .90 100 110 120 Abundance #292; N-Ethylformamide | . 30 7.00 7.20 7.40 7.60 7.80 73 m/z 71.1 " 5000 44 58

lil 15.11,4 44— — i ■ ■ ' ■ i ' 1 ■ ■ i ' ' ■ ' i ' — ————— m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.00 7.20 7.40 7.60 7.80

102.D GCMS0208.M Fri Feb 08 13:37:13 2002 Page 1

NYC-WTC_000050106