GCMS sample analysis results, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\30313.D Vial: 14 Acq On : 22 Dec 2001 7:31 pm Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 4.51. ug/1 1284370 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-DioxoZane, 2-methyl- 88 C4H802 000497-26-7 9 2 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 1,3 -Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 278 (7.600 mln): 30313.D (-) m/z 72.95 100.00% 73

5000- 43 • i ■ 1 ■ ■ i ■ 1 1 • i 1 1 1 ‘Tri i ■ i i i 87 103 7.20 7.40 7.60 7.80 8.00 38 |, | 50 55 61 67, । 1• i ■ ' 1 1 i ' ' ■ ■ i 1 ■ ■ ■ i ■ ‘ m/z 43.05 30.93% miz-> 10 20 __ 30 40 50 _ 60 70 80 90 100 110 Abundance #62902: 1,3-Dioxolane, 2-methyl- 73

5000 43 1 i 1 1 7.20 7.40 7.60 7.80 8.00 58 m/z 45.05 11.05% 87 j 27 T I J-1 1 I 1 ] 11 r pH l I i ] r ■ ■ i ■ • ■ 1 । 1 mfz~> 10 20 30 40 50 60 70 80 90 100 110 Abundance :#62932; Silane, tetramethyl- 73 7 20 7.40 7.60 7.80 8.00 5000 m/z 41.00 10.35%

45 ! 15 53 59 । 88 ; ■ 1 I ‘ 1 ‘ ‘ I 1 ‘ i ■ ■ • • i ■ • • • t ■ ■ ■ ‘ i ' 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide • i • ■ ■ ■ i ■ ■ ■ r i ■ ■ ■ ■ i ■ ' ■ ■ i • ■

33 7.20 7.40 7.60 7.80 8.00 73 m/z 71.00 6.79% 5000 44 58

...1. ■ • i ■ i ■ 1 — .. . 1 * 1* I * .

m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30313.D GCMS1126.M Wed Jan 02 10:17:07 2002 Page 1

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