GCMS analysis results for sample AD29523, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\29523.D Vial: 37 Acq On : 29 Dec 2001 12 :10 am Operator: 209 GALOS Sample : GC/MS SCAN 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1,3-Dioxolane, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.61 2.72 ug/1 1343280 1,4-Dichlorobenzene-d4 11.68

Hit# of 5. Tentative ID MW MolForm CAS# Qual

1 1,3 -Dioxolane , 2-methyl- 88 C4H802 000497-26-7 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 1,3 -Dioxolane , 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance 7 Scan 280 (7.612 min): 29523.D (-) m/ z 73.00 100.00%| 73

5000 43 । |........... 87 .............. 103............. 7.20 7.40 7.60 7.80 8.00 38 |, | 50 55 61 67, 1 I ' ' ' ' I ' ' ' ' I ' > | • > > ' | . । । । । ■ T ■ . । m/z 43.05 31.89% miz-> 10 20 . 30 40 50 60 70 80 90 100 110 'Abundance #62902: 1,3-Dioxolane, 2-methyl- 73

5000- 43 I 7.20 7.40 7.60 7.80 8.00

z...1.. I 58 m/ z 45.05 11.78% 1 87 L m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73 1 1 1 ■ 1 i ' 7.20 7.40 7.60 7.80 8.00 5000 - m/ z 41.00 11.13% 44 58 I 15 I .1 i i ' ■ ■ ■ i i ■ ■ ■ ■ । ' 9il ■ ■ i ' ■ ' 1 I 1 1 1 TI 1 I ■|"l"l miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- TpTTT, 7 ri 1 1 1 1 1 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.0.0 6.96% 5000

45 15 m/z-> TT 1 ' 'I ' 1 10 20 .......... —5359 ...... 30 40 50 60 70 80 88 90 100 110 7.20 7.40 7.60 7.80 8.00

29523.D GCMS1126.M Tue Jan 08 12:09:24 2002 Page 1

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