GCMS analysis results for sample AD29523, Jan 2002

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GCMS analysis report for sample AD29523 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036798–000036814

Folder label: “GCMS X 12/7/01 A 1/2/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\29523.D Vial: 37 Acq On : 29 Dec 2001 12:10 am Operator: 209 GALOS Sample : GC/MS SCAN 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K. L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

11.13 0.71 ug/1 351051 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 64 2 Benzene, 1-phenyl-4- (2-cyano-2-phen 281 C21H15N 027869-56-3 50 3 2-0xo-4-phenyl-6- (4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 4 2(1H)-Pyrimidinone, 5-chloro-4,6-di 282 C16H11C1N2O 028567-83-1 7 Abundance Scan 663 (11.128 min): 29523.D (-) m/ z 281.00 100.00% 281

5000 - — 73 133 193 -- 249 265 10.80 11.00 11.20 11.40 • ■ i 45 59 | 88 103 119 | 147 163 1771 207 > ‘i ■ • ■ ■ । ■ । ■ । । '' ■ > , '| ■' ■ • ■ । ■ ■ ■ ■ । ■' 24 5 1., I,, ■ 1 i ' ' 1 ' i ■ 1 m/z 282.00 29.37% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

5000 10.80 11.00 11.20 11.40 m/ z 283.00 18.94% 4 133 .. 207 . - ! ......... 73................|...... 163 177 191 |...... 235 249 265 , | miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 'Abundance #39643: Benzene, 1-phenyl-4-(2-cyano-2-phenylethenyl) 281 i ■ 1 i ■ ■ ■ ■ i 10.80 11.00 11.20 11.40 5000 - m/ z 133.00 12.03% 20s 253 ......................... . 1 126 203I 2 11 224 240 266 || ! I mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 281 10.80 11.00 11.20 11.40 m/z 192.90 11.88% 5000-

122 123 141— , 175 , TIPugmt 204 247 ■ 4 T T 11 __ T’ ' i ■ ■ ' ■ i ■ ' ‘ ‘ i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40

29523.D GCMS1126.M Tue Jan 08 12:09:28 2002 Page 2

NYC-WTC_000036806

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NYC-WTC_000036806Source: NYC Law Department, mirrored locally

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