GCMS analysis results for sample AD30357, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.

NYC-WTC_000017748–000017769

Folder label: “GCMS X 12/13/01 A 12/27/01”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2 701\30357.D Vial: 18 Acq On : 28 Dec 2001 4:40 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 11.13 0.50 ug/1 160996 1,4-Dichlorobenzene-d4 11.68 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H2404Si4 000556-67-2 86 2 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 25 3 2-Oxo-4-phenyl-6-(4-chlorophenyl) -1 282 C16H11C1N2O 000000-00-0 9 4 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 Abundance Scan 663 (11.128 mln): 30357.D (-) rn/z 281.00 100.00% 201

5000 TTIB**131—63E—CB—1 45 59 73 89 103 119 123 147 163 177 123 207 221 235 24% 225 10.80 11.00 11.20 11.40 1—ann———naatu’m—mmmmommmmTTTTTT. +rr m/z 282.0 J 26.95% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

5000 ‘ * i 11 > "• i 1 ' ■ • i * ■ * • i 10.80 11.00 11.20 11.40 m/z 283.00 16.16% 73 133 163 177 1?1 227 235 249 265 I ■ • i ■ ■ ■ • i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ • ■ ■ i ■ ■ ■ • i ■1 ■ • i1 ■ ■ 1 i ■ ■ • • i ■ ■ ■ ■ i1 ■

miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643; Benzene, 1-phery!-4-(2-cyanc-2-phenylethenyi) 281 - 10.80 11.00 11.20 11.40 5000 m/z 192.90 13.30% 253

miz-> 40 60 126

80 100 120 140 160 180 200 220 240 203 I; 224 240 .26.1 260 280 Abundance #39756:2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 281 10.80 11.00 11.20 11.40 ‘ ‘ m/z 133.00 11.12% 5000

102 123 141 175 204 247 * ■ i ' ■ ■ ■ i 1 •' ■ i • ■'' i1 **4iti 114,4,141**14." TTTTITTT 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40T1

30357.D GCMS1126.M Wed Jan 02 11:00:04 2002 Page 2

NYC-WTC_000017756

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NYC-WTC_000017756Source: NYC Law Department, mirrored locally

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