GCMS analysis results for sample AD30357, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC2 701\30357.D Vial: 18 Acq On : 28 Dec 2001 4:40 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

11.44 0.49 ug/1 159488 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy- 1-methylet 148 C7H16O3 020324-32-7 72 2 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H1403 000106-62-7 59 3 2-Propanol, 1,1’-[(1-methyl-1,2-eth 192 C9H20O4 001638-16-0 40 4 2-Propanol, 1,1' -oxybis- 134 C6H14O3 000110-98-5 39 Abundance Scan 697 (11.440 min): 30357.D (-) m/z 59.05 100.00% 59 45 5000- 73 103 ‘ I‘‘*I‘-IS**1**I 11.20 11.40 11.60 11.80 ... B 51 -m

N 1IT ‘1 > . . > I’m . i ■ ' ■ ■ i ■ m/z 44.95 51.86% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 45 73 103 11.20 11.40 11.60 11.80 31 m/z 103.05 30.34% ----- 130 ' I • • *111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #6086: 1-Propanol, 2-(2-bydraxypropoxy)- 59 11.20 11.40 11.60 11.80 5000 m/z 41.05 26.20% 31

NN 45 103 I 75 89 miz-> 20 30 " 40 sb' 60 70 80 90 100 110 120 130 Abundance #20630:2-Propanol, 1,1'-[(1-methyl-1,2-ethanedlyl)bis(oxy) i ‘ 59 11.20 11.40 11.60 11.80 m/z 73.00 24.76% 5000

m/z-> 20 , 31

40 45 , 73 ' I ' ‘ 1 ‘ I ' 1 1 ''l I 1 ' • i 1 ■ ' ' 1 1 ■ ■ ' i 11 ‘ ■ i ■ ‘ 30 391 50 60 70 80 ' i ‘ 90 103 , ' ■ i ‘ 1 ‘ ' i ‘ 1 100 110 117 i ■ ‘ 120 ' i ‘ ' 130 A MJ11.20 1140 11.60 11.80 '

30357.D GCMS1126.M Wed Jan 02 11:00:09 2002 Page 3

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