Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\FEB1302\30648.D Vial: 14 Acq On : 14 Feb 2002 3:48 am Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
11.74 1.92 ug/1 635623 1,4-Dichlorobenzene-d4 12.35
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 78 2 2-Oxo-4-phenyl-6- (4-chlorophenyl) -1 282 C16H11C1N2O 000000-00-0 9 3 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 4 Benzene, 1-phenyl-4<(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance Scan 730 (11.742 min): 30648.D(-) .. . . ... | m/z 281.0.0 100.00% 2! 11
5000 ... I ■ ■ i ■ ■ > ■ । ■ 1 1 1 1 ' ' i ' ‘ 1 45 59 73 89 103 119 133 147 163 177 1 207 221 235 249 265 11.40 11.60 11.80 12.00 1 I 1 ' ' I 1 ' 1 ■ I ‘ ' I 1 m/ z 2 82.00 28.33% m/Z-? 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281
... .................................... 5000 11.40 11.60 11.80 12.00 m/z 283.00 16.40% 73 133 -tai 207 | 163 177 191 J. 235 249 265 m/z->40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance r390t 2 dammphony)-d (4.. oi . n * 281 ....... I ' 1 I ' 1 1 1 I ' ‘ 1 118.4 11 1 11.40 11.60 11.80 12.00 5000 m/z 192.90 14.04%
102 -|23 141 175 204 247 ‘ i ■ ‘ ' i ' ■ ' ' i ' ' 1 ' i ' 1 ■ ' i ■ ' ' ' i 1 ' ■ 1 i 1 1 ■ ■ i ' ' ' ' i ‘ ' 1 ' i ' ' ' ' i m/z->40 60 80 100__120.. 140..160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5, 5-dioxide ■ ■ i ' 1 ■ ' i ' ‘ 1 1 i ■ ' ■ I 281 11.40 11.60 11.80 12.00 m/ Z 73 . Q0 8.87% 5000 217
m/z~> 102 118 TITIIPTTITTTmTTTII 40 60 80 232 189 294 „ lli 252264 li 100 120 140 160 180 200 220 240 260 280 .... / ' ' I ' ' 1 A 1 1 l ■ ' ■ > I 11.40 11.60 11.80 12.00
30648.D GCMS0103.M Thu Feb 14 11:01:25 2002 Page 2
NYC-WTC_000004479
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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