Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\FEB1302\30648.D Vial: 14 Acq On : 14 Feb 2002 3:48 am Operator: 209 GALOS Sample : GC/MS SCAN Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 HH-Dibenzo [b, E] [1,4] diazepin- Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.94 2.52 ug/1 1068280 Naphthalene-d8 16.00
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 HH-Dibenzo [b,E] [1,4] diazepin-11-on 267 C16H17N3O 013450-73-2 41 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 40 3 Benzoic acid, 2,6-bis [Atrimethylsil 370 C16H30O4S13 003782-85-2 37 4 Benzoic acid, Abundance 2-[Scan(trimethylsilyl) ox 282 C13H2203Si2 1078 (14.937 min): 30648.D (-) 003789-85-3 32 m/ z 73.00.. 100.00% 73
5000 267 355
45 133 154 177193 223 251 14.60 14.80 15.00 15.20 h 103 I || 293 323339 1 TIOITumuf i ■ " ■ i1 ■ I ■' i''''' 1" '' il ' Ti i it« 1 tint । i| '11■ ' i " " i " " i'11"'I' " 1 i'' ■ TI m/ z 2 66.90 46.65% m/z-2... 20 40 6080 100120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #37180: 11H-Dibenzo[b,Ej[1,4jdiazepin-i l -one, 5-(3-aminopro 30 1 8 77 267 181 223 .................. ,,................... 5000 249 14.60 14.80 15.00 15.20 52 m/z 355.05 31.47% I " ' ‘ i " " I ‘■ r " ' i " ■' i " " i " ‘111 ■'11" ' ■ i11 ■' I " " i " " 111" i'1 ■111' ■' r " 11'1'' i' " ' i m/z->20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance 73
355 14.60 14.80 15.00 15.20 267 5000 m/ z 267.90 12.70%
191207 251 323339 ; i1' ■' i " " 1" '11 " " i " " i' ■ " i ■' " i " " i " " i' ‘ " i " " i " " i ■ 1IIG m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet ................................................... 73 355 14.60 14.80 15.00 15.20 m/z 356.05 11.08% 5000
147 267 249 ....... 47........ ....................... , ................. : 208 i " ‘' i " " i " " r " ' i " " i " " i'1' ‘ i " " i " " i 1,7414.283, 111'' ’ l " " 111 I" " I ............................ ............. m/z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14-60 14.80 15.00 15.20
30648.D GCMS0103.M Thu Feb 14 11:01:29 2002 Page 3
NYC-WTC_000004480
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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