GCMS analysis results for sample AD30251, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30251.D Vial: 8 Acq On : 27 Dec 2001 6:58 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

14.31 0.55 ug/1 214784 Naphthalene-d8 15.28

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 3 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 37 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 1009 (14.308 min): 30251.D (-) m/ z 73.00 100.00% 73

5000 267 355 tdd1/d2////-d//"d/8/55/00//0/0/n.d 45 14.00 14.20 14.40 14.60 k. 89 108.133.154,|Trt177193 .. 223 IImuutn"//11147 25111A.i fi_i 2I—un*nna) 323339 t —aaananp m/z 266.90 35.98% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ‘ ’ 1 1 ‘ ' 1 1 ' 1 1 ' 1 14.00 14.20 14.40 14.60 m/z 355.05 26.39% 191207 251 323339 | m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol, tris(trimethylsily)- 73 ............. ................................... 14.00 14.20 14.40 14.60 267 m/z 267.90 5000 179 10.00% 356 45 147 . . 1 । 312 . 1 , ] . . 1 . । . .. . | ri 1 1 | 1 1 1 1 | 1 r 1 1 11 1 . . । .... । 209 237 । .. . j .... । .... । 1 . 1 4 .... j .... । miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls ■ • i ■ ■ ■ ■ i ■ ■ • ■ i 4 ■ • ■ i ■ • ■ ■ i i 73 14.00 14.20 14.40 14.60 355 m/ z 356.0 5 9.51% 5000

45 .4 179, .. 207223, . 267282, ............. .1...... miz-> 40 60 80 100 120 140 160 180 '266' 220 240 260 280 366' 320 340 360 ' 14.00 14.20 14.40 14.60

30251.D GCMS1126.M Wed Jan 02 10:38:30 2002 Page 3

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