GCMS analysis results for sample AE00009, Feb 13 2002

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Laboratory report documenting GCMS analysis of sample AE00009 with detection of unknown compounds and surrogate recovery.

NYC-WTC_000050122–000050134

Folder label: “GCMS X 1/3/02 A 1/24/02”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\l\DATA\JAN2402\9.D Vial : 11 Acq On : 24 Jan 2002 10:52 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Cyclopentasiloxane, decamethyl Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

14.13 0.64 ug/1 263113 Naphthal ene-d8 15.08

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 80 2 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40 3 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 990 (14.132 min): 9.D (-) m/z 73.00 100.00% 73

5000 267 355 tBT - T 45 251 13.80 14.00 14.20 14.40 I । । 103118133 154 177 193208223 323339 h miz-> 11r'■11' 40 60 IT’ i p-i i q-n rTTu‘"T‘ . ‘ । iTi 1Tr . p . TH TVOTETui 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 m/z 267.00 37.30% 'Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000- T 13.80 14.00 14.20 14.40 m/z 355.0,5 26.29% 251 323339 1 ‘ I‘ T‘rT‘0"TTTTTTTIT 191207 । ■11' ।11' I -mi- TITITPTT m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 [Abundance #51296: Benzoic acid. 2.6-bis[(trimethylsilyl)oxy]- trimet 73 355 \ TT 13.80 14.00 14.20 14.40 5000 m/z 356.0,5 9.72% 147 267 J 47 208 249 1 283 370 ' r " p > i > । , . . , । rk . rp . > > p t . . p > . < । p । . . . p .Ti p-n KITTuTT 11' ■11 m/z-> i ■'' ■ i 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ________ 'Abundance #49868: 3.4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 13.80 14.00 14.20 14.40 m/z 267.90 9.22% 267 5000 179 356 45 147 I . j • ■r' j ■ ■ I‘7l4 ‘‘I TuTTi 209 237 rv'■i " ■11 '• ■ 312 341 . j m . TTvsfTu m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 13.80 14.00 14.20 14.40

9.D GCMS0208.M Fri Feb 08 13:44:57 2002 Page 5

NYC-WTC_0000501 33

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GCMS analysis results for sample AE00008, Feb 13 2002 · Box DEP Box 28

NYC-WTC_000050109

Laboratory report documenting GCMS analysis of sample AE00008 with detection of unknown compounds and surrogate recovery.

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