NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30708.D Vial: 49
Acq On : 30 Dec 2001 6:21 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.31 3.50 ug/1 2032050 Napht halene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53
2 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40
3 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38
4 Benzeneethanamine, N- [ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 38
Abundance Scan 1009 (14.309 min): 30708.D (-) m/ Z 73.00 100.00%
i 73
5000-
267
355
TTu 1 । 'i 1 1 1 ■I
45 i 89 108 133 154 177 193208223o 251 14.00 14.20 14.40 14.60
- L 293 323339 J
- TmmumeummmmumaagaTBI1m001111710n1—OT1TT ‘T m/z 267.00 36.95%
m/z-> ____ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267
5000 i 1 ■ ■ ■ i ' ■ ■ 1 i
14.00 14.20 14.40 14.60
m/z 355.05 29.56%
. . 191207 251 I 323339
" I'' " i'''' । । ■ ■ ■ ■ ।।। । ।'111" 11111' 11 11111 mmPTTTTT
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #5 1296: Benzoic acid, 2,6-bis((trime’hylsilyloxyl- trimet
73 355
14.00 14.20 14.40 14.60
5000 m/z 356.05 10.29%
147 267
47 208 249 ; 283 370
m/z-> ■ I'''
40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #49868: 3,4-Dihydroxybenzy! alcohol,tris(trimethylsily!)-
73 14.00 14.20 14.40 14.60
m/z 267.90 9.72%
267
5000- 179
356
45 147
209 237 341 1,
TTTTT
" I " " I " " I " " I " 111 TTrp * vvnusls 11 " i11" i "312
" i ■' " f" "I 1 ‘ “ i
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
30708.D GCMS1126.M Mon Jan 28 11:28:32 2002 Page 4
NYC-WTC_000004343
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