GCMS analysis results for sample AD30016, Jan 2002

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Gas chromatography-mass spectrometry report documenting analysis of sample AD30016 conducted on January 28, 2002.

NYC-WTC_000037244–000037254

Folder label: “GCMS X 12/11/01 A 12/18/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\JAN1502\30016.D Vial: 25 Acq On : 15 Jan 2002 3:49 pm Operator: 209 GALOS Sample : gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 14.14 0.26 ug/1 127420 Naphthalene-d8 15.10 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H30O5Si5 000541-02-6 72 2 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 47 3 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 43 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 Abundance Scan 991 (14.145 mln): 30016.D (-) m/ z 73.00 100.00% 73

5000 267 355 TLI—E—.T TI’EET r-r-r-r-r.- r-m-p

miz-> m 45 115 133 154 177 193 223 251 1 TTTm TIT ■ ■ r IT. T TTTTMTTHTT rrrp-TTTp-rr 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 323339 t 13.80 14.00 14.20 14.40 m/z 267.00 .29.86% Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 5000 267 £ 1—AGIIETOIB —r. !1‘CE=TEE 13.80 14.00 14.20 14.40 m/z 355.05 27.58% 191207 251 . 323339 1‘1081109001—00m00110010000100010TTa". T ■i'■■ • i ■1 111111 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73978: Benzoic acid. 2.5-bis(trimethylsiloxy)- trimethyls 73 355 -------- 13.80 14.00 14.20 14.40 5000 m/z 356.05 8.84% 45 147 179 207223 267282297 , 370 i •i■• TTTTIi•<> i T TIUTIT miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868:3 ’0) • is(trimethyisilyl)- ‘ 1 I • • ‘ I ‘ ‘ ‘ l ■ ' ‘ • I 1 1 1 1 I 1 73 13.80 14.00 14.20 14.40 m/z 267.90 7.93% 267 5000- 179 356 45 147

miz—> iii | # j « J 11 j» t » )। I i i i | i » —t 209 237 , 312 341 | IIUOTTTTIT TITfnu I"‘ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 II ' 1 I • » » » I • » • » I ’ • ’ • | * * » > j । 13.80 14.00 14.20 14.40

30016.D GCMS1126.M Fri Jan 18 14:50:27 2002 Page 3

NYC-WTC_000037253

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NYC-WTC_000050145

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