GCMS analysis results for sample AD30016, Jan 2002

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Gas chromatography-mass spectrometry report documenting analysis of sample AD30016 conducted on January 28, 2002.

NYC-WTC_000037244–000037254

Folder label: “GCMS X 12/11/01 A 12/18/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\JAN1502\30016.D Vial: 25 Acq On : 15 Jan 2002 3:49 pm Operator: 209 GALOS Sample : gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

10.98 0.31 ug/1 121430 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 86 2 Benzene, /-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 50 3 2 (1H) -Pyrimidinone, 5-chloro-4,6-di 282 C16H11C1N2O 028567-83-1 9 4 2-Oxo-^r-phenyl-6-(4-chlorophenyl)-! 282 C16H11C1N2O 000000-00-0 9 Abundance Scan 646 (10.978 mln): 30016.D (-) i i ~~ m/z 281.00 100.00% 281

5000

10.60 10.80 11.00 11.20 11.40 .. 45 .59 73 86103 119 123 147 163 177 13 207 ... 235 249 265 ■ I . qi. . . I . . . > । ... i p. TTT . . . . । ... . । . . . .j . ... । .T. । । . ... । i . . . । . . . i |T m/z 282.00 28.16% miz-? 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

T 5000 T T 10.60 10,80 11.00 11.20 11.40 m/z 283.00 16.97% ...........73......... J3..... 163 177 191 T 235 249 265 L miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39643: Benzene, l-phenyl-4-(2-cyano-2-phenytethenyl) 281 10.60 10.80 11.00 11.20 11.40 5000 m/z 192.90 12.40% 126 203 253 J 224 240 J 266 l • ‘ I ‘ ‘ ‘ .1 ’ • ‘ ‘ l ‘ ‘ ‘ 110111 TT UBB—81111111183 JTT . ■ i > ■ l . | 4, m/z-2 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance............ #39758:2(1H)-PyrimWlnone, 5-chloro-4,6-diphenyl- 11 T TTT J T I TTTTT I J I I TT T 1— 281 10.60 10.80 11.00 11.20 11.40 m/z 133.00 10.48% 5000 77 104 247 204 T-r-p-i i ; । i r-rf | . . ‘ 1 i » | i i i i i i i i » । i : i i j : I I « । l i l Tyr '11 '111 i1 • | • • • • | • 4 • j • > > ‘ | rr-r-r-j-r- 40 60 80 100 120 140 160 180 200 220 240 260 280 10.60 10.80 11.00 11.20 11.40

30016.D GCMS1126.M Fri Jan 18 14:50:22 2002 Page 2

NYC-WTC_000037252

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NYC-WTC_000050145

Laboratory report documenting GCMS analysis of sample AE00107 with detection of unknown compounds and surrogate recovery.

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