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GCMS analysis results for sample AD30356, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30356 conducted on January 10, 2002.

NYC-WTC_000017770–000017781

Folder label: “GCMS X 12/13/01 A 12/27/01

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Scanned page image, NYC-WTC_000017779
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30356.D Vial: 21 Acq On : 28 Dec 2001 7:34 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 14.31 0.50 ug/1 204572 Naphthalene-d8 15.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 78 2 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40 3 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38 4 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 Abundance Scan 1009 (14.310 mln): 30356.D (-) m/ z 73.00 100.00% 73

5000 267 355 . 1 . । . TT -m- PrT 1 | I 1 I > J 45 14.00 14.20 14.40 14.60 108’133 -"I i ■ “111144 154 177 193208223 251 293 323339 1 4 ri [masr’s Ti ITTtaan . ."r. 1 M——upuanuuT m/z 267.00 37.06% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 14.00 14.20 14.40 14.60 m/z 355.05 30.06% 323339 | 191207 251 TImmmamuTummaOmmmn —nmOftI m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51296: Benzoic acid. 2.6-bis[(trimethvisilyl)oxy]-. trimet 73 355 1 ' I 1 ' 1 ' I 14.00 14.20 14.40 14.60 5000 m/z 268.00 11.08% 147 267 47 208 249 1 283 | 370 m/z-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ' #49868: 3,4-DihydroxybenzyI alcohol,tris(trimethylsilyl)- ■ ■ i • ' ‘ ■ i ■' ■ ' i ■ ‘ ■ i ■ ■ ■ ■ i i 73 14.00 14.20 14.40 14.60 m/z 356.05 9.92% 267 5000 179 356 45 147 209 237 , I 312 341 Tm0mn/mmnmmnu2B—ngmn—mCmug09 “ i ■ “ ■ i • “ ■ i • ■ rl “ “ i ■ ■ । ■ ■ ■' ।11 । • ■ ■ ■ । miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60

30356.D GCMS1126.M Wed Jan 02 10:57:14 2002 Page 3

NYC-WTC_000017779

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NYC-WTC_000017779Source: NYC Law Department, mirrored locally

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