NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30356.D Vial: 21
Acq On : 28 Dec 2001 7:34 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
14.31 0.50 ug/1 204572 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 78
2 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40
3 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38
4 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38
Abundance Scan 1009 (14.310 mln): 30356.D (-) m/ z 73.00 100.00%
73
5000
267
355 . 1 . । . TT -m- PrT 1 | I 1 I > J
45 14.00 14.20 14.40 14.60
108’133
-"I i ■ “111144 154 177 193208223 251 293 323339 1
4 ri [masr’s Ti ITTtaan . ."r. 1 M——upuanuuT m/z 267.00 37.06%
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267
5000
14.00 14.20 14.40 14.60
m/z 355.05 30.06%
323339 |
191207 251
TImmmamuTummaOmmmn —nmOftI
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #51296: Benzoic acid. 2.6-bis[(trimethvisilyl)oxy]-. trimet
73 355
1 ' I 1 ' 1 ' I
14.00 14.20 14.40 14.60
5000 m/z 268.00 11.08%
147 267
47 208 249 1 283 | 370
m/z->
Abundance
40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 '
#49868: 3,4-DihydroxybenzyI alcohol,tris(trimethylsilyl)- ■ ■ i • ' ‘ ■ i ■' ■ ' i ■ ‘ ■ i ■ ■ ■ ■ i
i 73 14.00 14.20 14.40 14.60
m/z 356.05 9.92%
267
5000 179
356
45 147
209 237 , I 312 341
Tm0mn/mmnmmnu2B—ngmn—mCmug09 “ i ■ “ ■ i • “ ■ i • ■ rl “ “ i ■ ■ । ■ ■ ■' ।11 । • ■ ■ ■ ।
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
30356.D GCMS1126.M Wed Jan 02 10:57:14 2002 Page 3
NYC-WTC_000017779
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