NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30425.D Vial: 5
Acq On : 27 Dec 2001 3:04 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
14.30 2.31 ug/1 875272 Naphthalene-d8 15.28
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74
2 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40
3 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38
4 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 38
Abundance Scan 1009 (14.305 mln): 30425.D (-) m/ z 73.0,0 100.00%
73
5000
267
355
11111a* 11 । * > • i 1 tir> ।
14.00 14.20 14.40 14.60
mz->
m ,+..*,89,198,133.134,,177193,723.r2%1 TImn)uunn2—napuT m/z 267.00
45
40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
293 323339 1
TT 32.77%
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267
5000
14.00 14.20 14.40 14.60
m/z 355.0 24.69%
323339 j
191207 251 !
। ‘ ‘14 T‘mmnsummuu-u1II1111ET13u ****
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #51296: Benzoic acid. 2.6-bis[(trimethylsilyl)oxy]- trimet
73 355
11*4* 14* I I 4 414***[
14.00 14.20 14.40 14.60
5000 m/z 267.90 9.31%
147 267
47 208 249 i 283 ‘ 370
■ ।■ • ■• ।
“ i “ ‘111 ■ • i “ ■' I ■ ■ ‘ ■ i" “ i • “ ■ i “' * i' ■'11 ■"' i 1 • ■ i ■ “ ■ i “ ■ ■ i ■ ■1 ■ i ■ •I*’*•i
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- TCIndnnOmDTat
73 14.00 14.20 14.40 14.60
m/z 356.0 9.02%
267
5000 179
356
45 147
209 237 . 312 341
I TIpmp—TmoT ■ > i ■" ■ i1 ■ •11 “ u “ l1' “ I
»‘ I • “ ‘ I “ “ I “ “ I • ‘1 ‘ I “ “ I “ • ‘ 11 ‘• • ' i ■ ■ ‘ ‘ i ■ ■ ■ ’ i 1 1 1 1 I'1 1 1 1 )
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
30425.D GCMS1126.M Wed Jan 02 11:03:55 2002 Page 4
NYC-WTC_000017713
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