NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\30425.D Vial: 5
Acq On : 27 Dec 2001 3:04 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 5 Cyclohexasiloxane, dodecamethy Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.45 3.90 ug/1 1478710 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 45
2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22
3 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12
4 Pregnane-3,20-dione, 11-[ (trimethyl 462 C26H46N203Si 057305-27-8 9
Abundance Scan 1352 (17.454 mln): 30425.D (-) m/ z 73.00 1 00.00%
73
5000
341
147 429 17.20 17.40 17.60 17.80
45 , , 96 117 1 179 207225 251 281 311 L t 381399 1
i
’ ’’1’4* Tmmmmmptm ।..,, ।....!.. I.!. .1.11 m/z 341.00 3 3.79%
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #56711: Cyclohexasiloxane, dodecamethyl-
73
341
429
5000 T T T T
17.20 17.40 17.60 17.80
m/z 147.0.0 14.06%
117 I
147
207 267 311 [ |
....l....।..." ।...H....।....।.1..t....11...।....।....।....।....।....।..i.।.111p.
........1.
I.... I ■,.. I..., I.... 1.
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #48337:2H-1 4-Benzodiazepin-2-one, 7-chloro-1 3-dihydro-5-
73 341
17.20 17.40 17.60 17.80
5000 m/z 429.05 11.06%
45
91
| 116 146 227 269 315, I
Tnpumemmmmpppg
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance> #73587: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- ’ **I*’1**41*-II l '
73 239 17.20 17.40 17.60 17.80
m/z 342.00 11.05%
342
5000
45 133
211
'....) (... r . r. ।.... j... .t.।... !.... ■" ■i‘ ■ ■ ■ i mkh TCI—upak" I \_________
1 • i ■ ■ • ■ i ■ 1 1 ■ i ‘ • i 1 1
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
30425.D GCMS1126.M Wed Jan 02 11:04:00 2002 Page 5
NYC-WTC_000017714
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