Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
NYC-WTC_000017854–000017878Folder label: “GCMS X 12/13/01 A 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30252.D Vial: 22 Acq On : 28 Dec 2001 9:31 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Cyclohexasiloxane, dodecamethy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 17.45 7.14 ug/1 2906950 Naphthalene-d8 15.28 Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 36 2 2H-l,4-Benzodiazepin-2-one, 7-chlor 342 C18H19C1N2OS1 055299-24-6 22 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 16 4 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 Abundance Scan 1352 (17.453 min): 30252.D (-) m/ z 73.0,0 100.00% 73
5000 341 147 429 17.20 17.40 17.60 17.80 miz-> 0-n 45 mHH96 117. [ 179.. 207225 251 281 311 [ 1 397..... L 1un—mnu—m——nm—umU—_um—uCEDEuOTI l. |....!.... ।, .1. ।. 40 60 80 100120140160180200220240260280300320340360380400420 m/z 341.00 32.30% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 17.20 17.40 17.60 17.80 147 m/z 147.00 14.78% । । * i • H i.. ।. i i 1111 117 ., 1111 । 207 267 ! .I i. mnpm |iii>|iiii|iiit|tiiijii 311 I I............ । I • U • 11. 11 p.. I j 1. 11J • 11. JI 11IJIII * J• m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48337 21-1 4-Benzodiazepin-2one, 7-chioro-1 3-dihydro-5- 73 341 / 17.20 17.40 17.60 17.80 ' 5000 m/z 342.00 11.27% 45 : 91 , 116 146 315, 227 269 \ . i i I . . . . ( . . II! . . I . I .. H | n TImmpag B110—0999—3991B001—030331—BT1T mfz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylslloxy)t T Bij..... 73 17.20 17.40 17.60 17.80 m/z 325.00 10.70% 147 5000 267 355 429 45 207
“ ' I ‘‘ ’ -rrrrprTTTyrTTTp-n^rjri-rTp^ I . TIWWTLWWTTNTTTTT \ I 11 ] I I TTfrrrrpTrrp-frrjT miz-> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
30252.D GCMS1126.M Wed Jan 02 10:42:23 2002 Page 5
NYC-WTC_000017866
OCR can misread numbers and units. Confirm readings against the page image before using them.
Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036614
Laboratory comments on GCMS scan results for sample AD29466 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000017649
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
Filed in the same folder
NYC-WTC_000017650
Laboratory log recording extraction parameters and sample counts for environmental samples processed in December 2001.
Filed in the same folder
NYC-WTC_000017654
Document showing calibration results for GCMS analysis of volatile organic compounds on December 27, 2001.
Filed in the same folder
NYC-WTC_000017658
Laboratory report documenting gas chromatography-mass spectrometry reference material analysis conducted on December 31, 2001.
Filed in the same folder
NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
Filed in the same folder