Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30710.D Vial: 48 Acq On : 30 Dec 2001 5:23 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclohexasiloxane, dodecamethy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.45 2.92 ug/1 1591910 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 36 2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 16 4 Silane, [1,2,3/-benzenetriyltris (oxy 342 C15H3 0O3Si3 017864-23-2 12 Abundance Scan 1352 (17.455 min): 30710.D (-) m/z 73.00 100.00% 73
5000 341 147 429 17.20 17.40 17.60 17.80
m/z-> 0 mhTpumg 45 , 96 117 179 207225 251 281 311 . —[ nudunu ’uT 40 60 80 100120140160180200220240260280300320340360380400420 397 . 111111 r11« n! ।! m/z 341.00 33.69% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
429 5000 17.20 17.40 17.60 17.80 147 m/z 147.00 14.67% 117 | 207 267 311 pojoha **) TTi . । > > > > । . > . . | i \ i i j I i i i | i . . > | i > i . | . > > . | > > H | TT TTp- m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48337; 2H-1.4-Senzodiazepin-2-one, 7-chloro-1 3-dihydro-5- 73 341
17.20 17.40 17.60 17.80 5000 m/z 342.00 10.93% 45 91 I 1 116 146 227 269 315 m/z-> ____ 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t . ....... H.......... 73 17.20 17.40 17.60 17.80 m/z 325.00 10.73% 147 5000 267 355 429 45 207
" " r"' i" " i" " r ■ ■ ■ r1 L.........I i..... Wg—T m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 17.20 17.40 17.60 17.80
30710.D GCMS1126.M Mon Jan 28 11:36:15 2002 Page 3
NYC-WTC_000004288
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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