Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C: \HPCHEM\ 1 \DATA\DEC2 70130710.D Vial: 48 Acq On : 30 Dec 2001 5:23 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
14.31 1.39 ug/1 761049 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 64 2 3i4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 3 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40 4 N-(Trifluoroacetyl)-O,01,011-tris(t 481 C19H34F3NO4Si3 000000-00-0 38 Abundance Scan 1009 (14.306 min): 30710.D (-) m/z 73.00 100.00% 73
5000 267 355 .............. ........... .................. .. 45 14.00 14.20 14.40 14.60 ' I i , 88 103 133 154 177193 223 251 1 293 323339 1 Th’uunmumumgT 111'111' 11 1 111" i'1'11" 1'111"T" ' ’ i " "i m/z 267.00 32.80% m/z-> 11111 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 14.00 14.20 14.40 14.60 m/z 355.0 24.97% 191207 251 323339 I 1 1 1 ‘ I TTTTTp-rrTp-rTTp-rTTyTTTTp-nTTTTTT-p-l^-TTTTTTp-TT^^ l1' " I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydraxybenzyl alcohol, tris(trimethysily)- 73 I ' ' ' ' I 1 1 ' ' I 14.00 14.20 14.40 14.60 267 5000 179 i m/z 356.05 9.08% 356 45 147 209 237 312 341 " ' 1111' I' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51296: Benzoic acid, 2,6-bls[(trimethylsilyl)oxy]-, trimet ‘ I’’ ■ ■ i ■ • ■ ■ । 73 355 14.00 14.20 14.40 14.60 m/z 267.90 8.81% 5000
147 267 47 '11 ‘ , I, 208>..... 1—2283 ’ I “ " I ’'' I ‘ “11111111'11111111111' THT I 249 370 11 in C| । 1 111* 11 p 11 ' I " " 11 “ 11'1 i ■i m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
30710.D GCMS1126.M Mon Jan 28 11:36:10 2002 Page 2
NYC-WTC_000004287
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
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