NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30252.D Vial: 22
Acq On : 28 Dec 2001 9:31 am Operator: 209 GALOS
Sample : GC/MS SCAN 12/13 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
14.30 3.56 ug/1 1449580 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50
2 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H32O3S13 068595-79-9 43
3 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40
4 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 38
Abundance Scan 1009 (14.304 mln): 30252.D (-) m/z 73.0,0 100.00%
73
5000
267
355
45 14'00 14'20 14.40 14.60 '
—0nnmuT ।223 dip r। ■ । 2. 93
, p ।, r 251
- iI00011
88 103 133 154 177 193 . 323339
M| I . I. |T. . .1 . ..T| 1. M1 m/z 266.90 31.95%
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267
5000
14.00 14.20 14.40 14.60
m/z 355.05 23.78%
191207 251 323339 ij
TTmm01m0100/m00m0122T83arr । ‘ i ■. “ i " i ■' ■ “ i •" ■ i
mfz~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #49868: 3,4-Dihydroxybenzyi alcohol, tris(trimethylsily!)-
73
267
14.00 14.20 14.40 14*60
5000 179 m/z 356.0 8.51%
356
45 147
Ii 312 341 209 237
l “ •‘I• • •‘I TTTIOTTTT
I ' ' ' ‘ I T T*TIO
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet
73 355 14.00 14.20 14.40 14.60
m/z 268.00 8.32%
5000
147 267
47... .............1 208!______ i. 249
L~ । A , 283 370 ................. ............................
i • ■ ■ ■ i ■ ■ ■ ‘ i ■1 •'' i “ ■ ■ i ■ " I'' " i ‘' i" ‘ TTTTTT
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
30252.D GCMS1126.M Wed Jan 02 10:42:18 2002 Page 4
NYC-WTC_000017865
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